4-溴-N,N-二乙基苯胺合成路线 (共 32 条)
反应条件
2,4,4,6-tetrabromo-3-n-pentadecylcyclohexa-2,5-dienone in cyclohexane T=20°C; 0.1 h;
参考文献
Attanasi, Orazio A.; Berretta, Stefano; Favi, Gianfranco; Filippone, Paolino; Mele, Giuseppe; Moscatelli, Giada; Saladino, Raffaele
Organic Letters, 2006 , vol. 8, # 19 p. 4291 - 4293
反应条件
dibenzo-18-crown-6; potassium bromide; copper(ll) bromide; 1,10-phenanthroline; copper(I) bromide in acetonitrile T=20°C; Sandmeyer bromination; 0.333333 h;
参考文献
Beletskaya, Irina P.; Sigeev, Alexander S.; Peregudov, Alexander S.; Petrovskii, Pavel V.
Synthesis, 2007 , # 16 p. 2534 - 2538
反应条件
copper(l) iodide; biphenyl-2-yl-di-tert-butyl-phosphane; lithium tert-butylate in 1,4-dioxane T=20°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Miki, Yuya; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2013 , vol. 15, # 1 p. 172 - 175
反应条件
1: 4-bromo-aniline With sodium hydride in tetrahydrofuran T=0°C; 0.5 h; 2: ethyl iodide in tetrahydrofuran T=20°C; 3 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 27 p. 9696 - 9697
反应条件
bis(1,2-diphenylphosphino)benzene; copper (II) acetate monohydrate; lithium tert-butylate in tetrahydrofuran T=20°C; Chan-Lam type coupling; 4 h; Inert atmosphere;
参考文献
Matsuda, Naoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3642 - 3645
反应条件
nitromethane; 2-iodosylbenzoic acid; [14C]-Tetramethylammonium bromide in tetrahydrofuran T=70°C; 3 h; regioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 77, # 1 p. 626 - 631
反应条件
PdCl2<(oTol)3P>2 in toluene T=100°C; 3 h;
参考文献
Kosugi, Masanori; Kameyama,Masayuki; Migita, Toshihiko
Chemistry Letters, 1983 , p. 927 - 928
反应条件
tetra-n-butylammonium tribromide in chloroform 0.0333333 h; Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 2061 - 2066
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in water T=0°C; bromination at various temperature; Product distribution;
参考文献
Tetrahedron, , vol. 50, # 12 p. 3797 - 3802
反应条件
tris(dibenzylideneacetone)dipalladium (0); tris-(o-tolyl)phosphine; sodium t-butanolate in 1,4-dioxane 20 h; Heating;
参考文献
Russian Chemical Bulletin, , vol. 47, # 7 p. 1416 - 1417