4-甲基-1-苯基戊烷-1-酮合成路线 （共 23 条）
反应条件
1.1: 92 percent / n-BuLi / tetrahydrofuran; hexane / 2 h / -50 - 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -50 °C 2.2: 94 percent / tetrahydrofuran; hexane / 1 h / -50 - 20 °C 3.1: 70 percent / aq. H2SO4 / benzene / 4 h / Heating View Scheme
参考文献
Grison, Claude; Thomas, Antoine; Coutrot, Frederic; Coutrot, Philippe
Tetrahedron, 2003 , vol. 59, # 12 p. 2101 - 2123
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -50 °C 1.2: 94 percent / tetrahydrofuran; hexane / 1 h / -50 - 20 °C 2.1: 70 percent / aq. H2SO4 / benzene / 4 h / Heating View Scheme
参考文献
Grison, Claude; Thomas, Antoine; Coutrot, Frederic; Coutrot, Philippe
Tetrahedron, 2003 , vol. 59, # 12 p. 2101 - 2123
反应条件
aluminium trichloride
参考文献
Urry,W.H. et al.
Journal of Organic Chemistry, 1964 , vol. 29, # 7 p. 1663 - 1669
反应条件
carbon disulfide; aluminium trichloride
参考文献
Thierfelder; Klenk
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1924 , vol. 141, p. 14
参考文献
Bamford, Anthony F.; Cook, Malcolm D.; Roberts, Brian P.
Tetrahedron Letters, 1983 , vol. 24, # 35 p. 3779 - 3782
反应条件
Reaktion ueber mehrere Stufen;
参考文献
Paterno; Traetta-Mosca
Gazzetta Chimica Italiana, 1909 , vol. 39 I, p. 452
反应条件
in methanol T=10°C; Irradiationdifferent concentration of trapping oxygen, lifetime; Product distributionKinetics;
参考文献
Adam, Waldemar; Grabowski, Sven; Wilson, R. Marshall
Chemische Berichte, 1989 , vol. 122, p. 561 - 564
反应条件
hydrogen selenide in methanol T=20°C; 24 h; Irradiation;
参考文献
Kambe, Nobuaki; Masawaki, Teruyuki; Kondo, Kiyoshi; Miyoshi, Noritake; Ogawa, Akiya; Sonoda, Noboru
Chemistry Letters, 1987 , p. 1907 - 1910
反应条件
1: toluene-4-sulfonic acid / toluene / 60 h / Molecular sieve; Reflux; Inert atmosphere; Dean-Stark trap 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.75 h / -78 °C / Inert atmosphere 3: [Ph3PCuCl]4 / tetrahydrofuran / 2 h / Reflux; Inert atmosphere View Scheme
参考文献
Motiwala, Hashim F.; Guelgeze, Belgin; Aube, Jeffrey
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7005 - 7022
反应条件
hydrogen selenide in methanol T=20°C; 24 h; Irradiation;
参考文献
Kambe, Nobuaki; Masawaki, Teruyuki; Kondo, Kiyoshi; Miyoshi, Noritake; Ogawa, Akiya; Sonoda, Noboru
Chemistry Letters, 1987 , p. 1907 - 1910
