苯并[b]萘并[1,2-d]呋喃合成路线 (共 28 条)
反应条件
potassium carbonate in 1-methyl-pyrrolidin-2-one T=150°C; Williamson ether Synthesis; 6 h; Inert atmosphere;
参考文献
US2012/165550 A1, ;
Page/Page column 17-18 ;
反应条件
[Ni0(1,5-cyclooctadiene)2]; caesium carbonate; dcype in anhydrous xylene T=160°C; 72 h;
参考文献
Tetrahedron, , vol. 69, # 27-28 p. 5780 - 5790
反应条件
2Ag(1+)*CH2O3(2-); Pd(TFA)2 in 1,4-dioxane; dimethyl sulfoxide T=150°C; 14 h; Inert atmosphere; regioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 131, p. 4194 - 4195
反应条件
palladium diacetate; caesium carbonate; CsO2CCMe3; dcype in anhydrous xylene T=140°C; 17 h; GloveboxSealed tube; Overall yield = 84 percent; Overall yield = 60.1 mg;
参考文献
Organic Letters, , vol. 14, # 18 p. 4838 - 4841,4
Organic Letters, , vol. 14, # 18 p. 4838 - 4841
反应条件
1: potassium carbonate / palladium diacetate / toluene; ethanol 2: potassium carbonate / water View Scheme
参考文献
US2012/165550 A1, ;
US2012/165556 A1, ;
反应条件
1: sodium carbonate / tetrakis (triphenylphosphine) palladium (0) / toluene; ethanol 2: boron tribromide; anhydrous sodium hydrogen carbonate / dichloromethane; water 3: potassium carbonate / water View Scheme
参考文献
US2012/165550 A1, ;
US2012/165556 A1, ;
反应条件
1: potassium carbonate / palladium diacetate / toluene; ethanol 2: potassium carbonate / water View Scheme
参考文献
US2012/165550 A1, ;
US2012/165556 A1, ;
反应条件
T=650°C; P=0.001 Torr; 1 h; Flash vacuum pyrolysis;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 13 p. 2961 - 2967
反应条件
1: NaBH4 / methanol; CH2Cl2 / 2 h / 20 °C 2: Pd-C / triethylene glycol dimethyl ether / 24 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 57, # 23 p. 4959 - 4965
反应条件
potassium tert-butylate in ammonia 3 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 33, # 17 p. 2323 - 2326