7H-吲哚并[2,3-c]喹啉合成路线 （共 29 条）
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium tert-butylate in N,N-dimethyl-formamide; toluene
T=100°C; 36 h;
参考文献
Zhang, Xiaoxia; Yao, Tuanli; Campo, Marino A.; Larock, Richard C.
Tetrahedron, 2010 , vol. 66, # 6 p. 1177 - 1187
反应条件
sodium acetate; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl acetamide
T=180°C; Heck reaction; 0.166667 h; microwave irradiation;
参考文献
Hostyn, Steven; Maes, Bert U.W.; Van Baelen, Gitte; Gulevskaya, Anna; Meyers, Caroline; Smits, Koen
Tetrahedron, 2006 , vol. 62, # 19 p. 4676 - 4684
反应条件
sodium acetate; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl acetamide
T=130°C; 48 h;
参考文献
Hostyn, Steven; Maes, Bert U.W.; Pieters, Luc; Lemiere, Guy L.F.; Matyus, Peter; Hajos, Gyoergy; Dommisse, Roger A.
Tetrahedron, 2005 , vol. 61, # 6 p. 1571 - 1577
反应条件
sulfuric acid; iodine in methanol; benzene
T=20°C; 48 h; UV-irradiation;
参考文献
Dhanabal; Sangeetha; Mohan
Tetrahedron, 2006 , vol. 62, # 26 p. 6258 - 6263
反应条件
1: 70 percent / 5 h / 200 °C
2: 51 percent / sulfuric acid; iodine / benzene; methanol / 48 h / 20 °C / UV-irradiation
View Scheme
参考文献
Dhanabal; Sangeetha; Mohan
Tetrahedron, 2006 , vol. 62, # 26 p. 6258 - 6263
反应条件
1: 45 percent / CuI; Et3N / PdCl2(PPh3)2 / 20 °C
2: 55 percent / NaHCO3; I2 / acetonitrile / 20 °C
3: 65 percent / dppf; t-BuOK / PdCl2(dppf) / toluene; dimethylformamide / 36 h / 100 °C
View Scheme
参考文献
Zhang, Xiaoxia; Campo, Marino A.; Yao, Tuanli; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 5 p. 763 - 766
反应条件
1: 45 percent / CuI; Et3N / PdCl2(PPh3)2 / 20 °C
2: 55 percent / NaHCO3; I2 / acetonitrile / 20 °C
3: 65 percent / dppf; t-BuOK / PdCl2(dppf) / toluene; dimethylformamide / 36 h / 100 °C
View Scheme
参考文献
Zhang, Xiaoxia; Campo, Marino A.; Yao, Tuanli; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 5 p. 763 - 766
反应条件
1: 55 percent / NaHCO3; I2 / acetonitrile / 20 °C
2: 65 percent / dppf; t-BuOK / PdCl2(dppf) / toluene; dimethylformamide / 36 h / 100 °C
View Scheme
参考文献
Zhang, Xiaoxia; Campo, Marino A.; Yao, Tuanli; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 5 p. 763 - 766
反应条件
1: 63 percent / Cu powder / Pd2(dba)3 / dimethylsulfoxide / 2 h / 80 °C
2: 66 percent / H2 / Pd/C / methanol / 10 h / 18 °C / 760 Torr
View Scheme
参考文献
Banwell, Martin G.; Lupton, David W.; Ma, Xinghua; Renner, Jens; Sydnes, Magne O.
Organic Letters, 2004 , vol. 6, # 16 p. 2741 - 2744
反应条件
1: 63 percent / Cu powder / Pd2(dba)3 / dimethylsulfoxide / 2 h / 80 °C
2: 66 percent / H2 / Pd/C / methanol / 10 h / 18 °C / 760 Torr
View Scheme
参考文献
Banwell, Martin G.; Lupton, David W.; Ma, Xinghua; Renner, Jens; Sydnes, Magne O.
Organic Letters, 2004 , vol. 6, # 16 p. 2741 - 2744
