对甲氧基-alpha-苯基苯乙醇合成路线 (共 17 条)
反应条件
1: With pinacol borane; 1,4-di(diphenylphosphino)-butane; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate in tetrahydrofuran
T=80°C; 72 h;
2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran
T=20°C; Further stages. Title compound not separated from byproducts.;
参考文献
Edwards, David R.; Hleba, Yonek B.; Lata, Christopher J.; Calhoun, Larry A.; Crudden, Cathleen M.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 41 p. 7799 - 7802
反应条件
4,4'-di(tert-butyl)-[1,1-biphenyl]yllithium in tetrahydrofuran
T=-78°C;
参考文献
Krief, Alain; Nazih, Abdesslame; Hobe, Myriam
Tetrahedron Letters, 1995 , vol. 36, # 44 p. 8111 - 8114
反应条件
lithium aluminium tetrahydride
参考文献
Huisgen; Ruechardt
Justus Liebigs Annalen der Chemie, 1956 , vol. 601, p. 21,31
反应条件
manganese in tetrahydrofuran
T=20°C; 0.0833333 h;
参考文献
Barrero, Alejandro F.; Herrador, M. Mar; Del Moral, Jose F. Quilez; Arteaga, Pilar; Akssira, Mohammed; El Hanbali, Fadwa; Arteaga, Jesus F.; Dieguez, Horacio R.; Sanchez, Elena M.
Journal of Organic Chemistry, 2007 , vol. 72, # 6 p. 2251 - 2254
反应条件
palladium 10 on activated carbon; hydrogen; acetic acid in ethyl acetate
T=20°C; P=760.051 Torr; 7 h; regioselective reaction;
参考文献
Blasio, Nadia Di; Lopardo, Maria Teresa; Lupattelli, Paolo
European Journal of Organic Chemistry, 2009 , # 6 p. 938 - 944
反应条件
dipotassium hydrogenphosphate; silver nitrate; zinc in water
T=30°C; 1 h;
参考文献
Bieber, Lothar W.; Storch, Elisabeth C.; Malvestiti, Ivani; Da Silva, Margarete F.
Tetrahedron Letters, 1998 , vol. 39, # 51 p. 9393 - 9396
反应条件
1: tetrahydrofuran
2: NaBH4 / propan-2-ol
View Scheme
参考文献
Baciocchi, Enrico; Bietti, Massimo; Putignani, Lorenza; Steenken, Steen
Journal of the American Chemical Society, 1996 , vol. 118, # 25 p. 5952 - 5960
反应条件
1: tetrahydrofuran
2: NaBH4 / propan-2-ol
View Scheme
参考文献
Baciocchi, Enrico; Bietti, Massimo; Putignani, Lorenza; Steenken, Steen
Journal of the American Chemical Society, 1996 , vol. 118, # 25 p. 5952 - 5960
反应条件
1: aqueous ethanol
2: tin; aq.-ethanolic HCl; CuSO4
3: sodium-amalgam
View Scheme
参考文献
Jenkins
Journal of the American Chemical Society, 1932 , vol. 54, p. 1155,1161
反应条件
oxygen in tetrachloromethane
14 h; Irradiation;
参考文献
Kakusawa, Naoki; Tsuchiya, Takashi; Kurita, Jyoji
Tetrahedron Letters, 1998 , vol. 39, # 52 p. 9743 - 9746