甲基 3-硝基丙酸酯 97合成路线 （共 11 条）
反应条件
KNO2; acetic acid in dimethyl sulfoxide T=15 - 18°C; 24 h;
参考文献
Miyakoshi, Tetuo; Saito, Shojiro; Kumanotani, Ju
Chemistry Letters, 1981 , p. 1677 - 1678
反应条件
sulfuric acid 8 h; Heating;
参考文献
Seebach, Dieter; Henning, Rainer; Mukhopadhyay, Triptikumar
Chemische Berichte, 1982 , vol. 115, # 5 p. 1705 - 1720
反应条件
hexamethyl-distannane in tetrahydrofuran Alkylation; Elimination; UV-irradiation;
参考文献
Kim; Yoon; Lim
Synlett, 2000 , # 8 p. 1151 - 1153
参考文献
Belikow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1956 , p. 855,858;engl.Ausg.S.875,877
参考文献
Birch,A.J. et al.
Australian Journal of Chemistry, 1968 , vol. 21, p. 2775 - 2784
Full Text Show Details
Sakai; Oida; Oki
Chemical and pharmaceutical bulletin, 1968 , vol. 16, # 6 p. 1048 - 1055
反应条件
ammonium formate; palladium on activated charcoal in methanol 0.166667 h; Ambient temperature;
参考文献
Ram, Siya; Ehrenkaufer, Richard E.
Synthesis, 1986 , # 1 p. 133 - 135
反应条件
Amberlyst A-21 in ethyl acetate
24 h;
参考文献
Ma, Jie; Wang, Si Hong; Guan, Rong Tian
Synthetic Communications, 2006 , vol. 36, # 9 p. 1229 - 1233
反应条件
Amberlyst A-21 in ethyl acetate
24 h;
参考文献
Ma, Jie; Wang, Si Hong; Guan, Rong Tian
Synthetic Communications, 2006 , vol. 36, # 9 p. 1229 - 1233
反应条件
Amberlyst A-21 in ethyl acetate
24 h;
参考文献
Ma, Jie; Wang, Si Hong; Guan, Rong Tian
Synthetic Communications, 2006 , vol. 36, # 9 p. 1229 - 1233
反应条件
1: methyl β-nitropropionate With N,N'-dimethyl-N,N'-propyleneurea; n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=-78°C; 0.5 h; Inert atmosphere;
2: ethyl iodide in tetrahydrofuran; hexane
T=-78 - 20°C; Inert atmosphere;
参考文献
Pelletier, Sophie M.-C.; Ray, Peter C.; Dixon, Darren J.
Organic Letters, 2011 , vol. 13, # 24 p. 6406 - 6409
