3,4-乙撑基二氧甲醛噻吩合成路线 （共 6 条）
反应条件
trichlorophosphate T=-10 - 20°C; 1.25 h;
参考文献
Firstenberg, Michal; Shivananda, Kammasandra Nanjunda; Cohen, Irit; Solomeshch, Olga; Medvedev, Vladislav; Tessler, Nir; Eichen, Yoav
Advanced Functional Materials, 2011 , vol. 21, # 4 p. 634 - 643
反应条件
N,N-dimethyl-formamide; trichlorophosphate T=-10 - 20°C; Vilsmeier formylation;
参考文献
Shivananda, Kammasandra Nanjunda; Cohen, Irit; Borzin, Elena; Gerchikov, Yulia; Firstenberg, Michal; Solomeshch, Olga; Tessler, Nir; Eichen, Yoav
Advanced Functional Materials, 2012 , vol. 22, # 7 p. 1489 - 1501
反应条件
n-butyllithium; potassium tert-butylate; lithium bromide 1.) THF, hexane, -90 deg C, 30 min, 2.) -90 deg c to room temperature; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 64, # 12 p. 4267 - 4272
参考文献
Chemical Communications, , # 33 p. 4187 - 4189
反应条件
N-bromosuccinmide in acetonitrile T=20°C; 60 h;
参考文献
Jessing, Mikkel; Brandt, Malene; Jensen, Knud J.; Christensen, Jorn B.; Boas, Ulrik
Journal of Organic Chemistry, 2006 , vol. 71, # 18 p. 6734 - 6741
反应条件
sodium tetrahydroborate in methanol
参考文献
Isidro-Llobet, Albert; Alvarez, Mercedes; Albericio, Fernando
Tetrahedron Letters, 2008 , vol. 49, # 20 p. 3304 - 3307
