2,3-二甲基-2,3-丁二胺合成路线 （共 38 条）
参考文献
Bieraeugel, H.; Plemp, R.; Hiemstra, H. C.; Pandit, U. K.
Tetrahedron, 1983 , vol. 39, # 23 p. 3971 - 3980
反应条件
hydrogenchloride in tetrahydrofuran; diethyl ether; hexane
参考文献
TRANSITIONS OPTICAL, INC.
Patent: US2012/156508 A1, 2012 ;
反应条件
in tetramethylene sulfide; diethyl ether
参考文献
Lilly Industries Limited
Patent: US4143047 A1, 1979 ;
反应条件
1.1: 92 percent / diethyl ether / ice cooling
2.1: m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 / 1 h / Ice cooling
2.2: aq. NaIO4 / CH2Cl2
View Scheme
参考文献
Hirel, Catherine; Vostrikova, Kira E.; Pecaut, Jacques; Ovcharenko, Victor I.; Rey, Paul
Chemistry - A European Journal, 2001 , vol. 7, # 9 p. 2007 - 2014
反应条件
1.1: 95 percent / diethyl ether / ice cooling
2.1: m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 / 1 h / Ice cooling
2.2: aq. NaIO4 / CH2Cl2
View Scheme
参考文献
Hirel, Catherine; Vostrikova, Kira E.; Pecaut, Jacques; Ovcharenko, Victor I.; Rey, Paul
Chemistry - A European Journal, 2001 , vol. 7, # 9 p. 2007 - 2014
反应条件
in tetrahydrofuran; water
参考文献
Eli Lilly and Company Limited
Patent: US5773448 A1, 1998 ;
US 5773448 A
参考文献
Sayre
Journal of the American Chemical Society, 1955 , vol. 77, p. 6689
反应条件
1.1: 95 percent / diethyl ether / ice cooling
2.1: m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 / 1 h / Ice cooling
2.2: aq. NaIO4 / CH2Cl2
View Scheme
参考文献
Hirel, Catherine; Vostrikova, Kira E.; Pecaut, Jacques; Ovcharenko, Victor I.; Rey, Paul
Chemistry - A European Journal, 2001 , vol. 7, # 9 p. 2007 - 2014
