2-苯基-1-丁烯-1-酮合成路线 （共 19 条）
反应条件
1: chiral (+)-ferrocene catalyst / CHCl3 / 22 h / 0 °C 2: 81 percent / H2O2; LiOH*H2O / tetrahydrofuran; H2O / 1.5 h / 0 °C View Scheme
参考文献
Wiskur, Sheryl L.; Fu, Gregory C.
Journal of the American Chemical Society, 2005 , vol. 127, # 17 p. 6176 - 6177
反应条件
1: With n-butyllithium; diethylzinc; (S)-(+)-3-hydroxy-tetrahydrofuran in hexane; toluene T=-78 - 0°C; 13 h; 2: With hydrogenchloride in tetrahydrofuran T=20°C; 48 h; Title compound not separated from byproducts;
参考文献
Tandon, Vishnu K.
Tetrahedron Letters, 2001 , vol. 42, # 34 p. 5985 - 5987
反应条件
in tetrahydrofuran T=-78 - 25°C; 2 h; Yields of byproduct given;
参考文献
Gong, Leyi; Leung-Toung, Regis; Tidwell, Thomas T.
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3634 - 3639
反应条件
in tetrahydrofuran T=-78 - 25°C; 2 h; Yield given;
参考文献
Gong, Leyi; Leung-Toung, Regis; Tidwell, Thomas T.
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3634 - 3639
反应条件
sulfur dioxide T=-261.2°C; Irradiationinvestigation of photoadducts; λ > 300 nm; Mechanism;
参考文献
Dunkin, Ian R.; MacDonald, J. Gavin
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 2079 - 2084
反应条件
1: With n-butyllithium; diethylzinc; (S)-(+)-3-hydroxy-tetrahydrofuran in hexane; toluene T=-78 - 0°C; 13 h; 2: With hydrogenchloride in tetrahydrofuran T=20°C; 48 h; Title compound not separated from byproducts;
参考文献
Tandon, Vishnu K.
Tetrahedron Letters, 2001 , vol. 42, # 34 p. 5985 - 5987
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=120°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 26, # 42 p. 5143 - 5144
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=120°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 26, # 42 p. 5143 - 5144
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=120°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 26, # 42 p. 5143 - 5144
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=120°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 26, # 42 p. 5143 - 5144
