2-氨基-3,5-二硝基噻吩合成路线 (共 3 条)
反应条件
sulfuric acid; water T=100°C; Deacetylation; 4 h;
参考文献
Yuquan, Shen; Yuxia, Zhao; Zao, Li; Jianghong, Wang; Ling, Qiu; Shixiong, Liu; Jianfeng, Zhai; Jiayun, Zhou
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 24 p. 3691 - 3695
反应条件
sulfuric acid
T=60°C; 0.5 h;
参考文献
Iddon, Brian; Khan, Nazir; Lim, Bee Lan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1457 - 1464
反应条件
1: With nitrosyl sulfuric acid; sulfuric acid; sodium nitrite; acetic acid; propionic acid
T=5°C; 0.75 h;
2: With water; hypophosphorous ether
T=20°C; Further stages.;
参考文献
Morley, John O.; Matthews, Thomas P.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 2 p. 359 - 366