N,N-双(2-溴乙基)苯胺合成路线 (共 7 条)
反应条件
phosphorus tribromide in dichloromethane T=0 - 20°C; 4.33333 h; Inert atmosphere;
参考文献
Dong, Qingchen; Rose, Michael J.; Wong, Wai-Yeung; Gray, Harry B.
Inorganic Chemistry, 2011 , vol. 50, # 20 p. 10213 - 10224
反应条件
sodium bromide in N,N-dimethyl-formamide T=80°C; 0.333333 h;
参考文献
Palmer, Brian D.; Wilson, William R.; Pullen, Susan M.; Denny, William A.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 112 - 121
反应条件
water; hydrogen bromide T=120°C;
参考文献
Cerkovnikov; Stern
Arhiv za Kemiju, 1946 , vol. 18, p. 12,24
Chem.Abstr., 1948 , p. 1938
反应条件
1: calcium carbonate; water 2: phosphorus (III)-bromide View Scheme
参考文献
Ross
Journal of the Chemical Society, 1949 , p. 183,184
反应条件
caesium carbonate in tetrahydrofuran Reflux;
参考文献
Atilgan, Serdar; Kutuk, Ilker; Ozdemir, Tugba
Tetrahedron Letters, 2010 , vol. 51, # 6 p. 892 - 894
反应条件
1: bis-diphenylphosphine With potassium tert-butylate in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: N,N-bis(2-bromoethyl)phenylamine in tetrahydrofuran T=0 - 20°C; 5 h; Inert atmosphere;
参考文献
Dong, Qingchen; Rose, Michael J.; Wong, Wai-Yeung; Gray, Harry B.
Inorganic Chemistry, 2011 , vol. 50, # 20 p. 10213 - 10224
参考文献
Cerkovnikov; Stern
Arhiv za Kemiju, 1946 , vol. 18, p. 12,24
Chem.Abstr., 1948 , p. 1938