1-叠氮基-2-甲氧基苯合成路线 (共 14 条)
反应条件
1: With sulfuric acid; sodium nitrite in water; acetic acid T=0 - 5°C; 0.166667 h; 2: With sodium azide in water; acetic acid T=0 - 5°C; 3 h;
参考文献
Heterocycles, , vol. 53, # 12 p. 2809 - 2819
反应条件
copper(l) iodide; sodium azide; L-proline; sodium hydroxide in dimethyl sulfoxide T=70°C; 24 h;
参考文献
Chemical communications (Cambridge, England), , # 7 p. 888 - 889
反应条件
sodium azide; copper(II) sulfate in methanol T=20°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 48, # 20 p. 3525 - 3529
反应条件
Cu(TMHD)2 in N,N-dimethyl-formamide T=100°C; 4 h; Sealed tube;
参考文献
Synthetic Communications, , vol. 44, # 3 p. 399 - 407
反应条件
sodium azide in dimethyl sulfoxide 3 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 721 - 722
反应条件
hydrogenchloride; water; sodium nitrite in diethyl ether T=0°C; 3 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 16, # 22 p. 9817 - 9829
反应条件
oxygen; nitrogen(II) oxide in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 53, # 46 p. 15701 - 15710
反应条件
sodium azide in 1,4-dioxane T=-15°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 4 p. 1047 - 1051
反应条件
sodium methylate in methanol
参考文献
Obushak; Pokhodylo; Pidlypnyi; Matiichuk
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 10 p. 1522 - 1527
反应条件
1: sodium ethoxide / ethanol 2: sodium hydroxide / H2O View Scheme
参考文献
Sun, Xiao-Wen; Xu, Peng-Fei; Zhang, Zi-Yi
Magnetic Resonance in Chemistry, 1998 , vol. 36, # 6 p. 459 - 460