1,2-二(苯基)丙-1-酮合成路线 (共 138 条)
参考文献
Ghera,E.
Journal of Organic Chemistry, 1970 , vol. 35, p. 660 - 666
参考文献
Ghera,E.
Journal of Organic Chemistry, 1970 , vol. 35, p. 660 - 666
反应条件
triethylsilane; tert-Butylmercury(II) chloride; sodium thiosulfate
1.) DMSO, 12 h, 2.) DMSO; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Russell, Glen A.; Shi, Bing Zhi; Jiang, Wan; Hu, Shuiesheng; Kim, Byeong H.; Baik, Woonphil
Journal of the American Chemical Society, 1995 , vol. 117, # 14 p. 3952 - 3962
反应条件
1: diethyl ether / Ambient temperature
2: Sarett reagent / oxydation
View Scheme
参考文献
Lasperas, M.; Perez-Rubalcaba, A.; Quiroga-Feijoo, M. L.
Tetrahedron, 1980 , vol. 36, p. 3403 - 3408
反应条件
1-methylcyclopentane; HUSY-zeolite
T=130°C; 15 h; sealed tube;
参考文献
Sani Souna Sido, Abdelkarim; Chassaing, Stefan; Kumarraja, Mayilvasagam; Pale, Patrick; Sommer, Jean
Tetrahedron Letters, 2007 , vol. 48, # 33 p. 5911 - 5914
反应条件
silver nitrate in ethanol
T=35°C; 2 h; Product distributionMechanism;
参考文献
Bach, Robert D.; Domagala, John M.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4181 - 4188
反应条件
oxygen; thiamine diphosphate in cyclohexane
1 h; Irradiation;
参考文献
Sawaki, Yasuhiko; Ishiguro, Katsuya
Tetrahedron Letters, 1984 , vol. 25, # 14 p. 1487 - 1490
反应条件
in diethyl ether
1 h; Ambient temperature;
参考文献
Kashima, Choji; Kita, Isanobu; Takahashi, Katsumi; Hosomi, Akira
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 1 p. 25 - 28
反应条件
1: (2R*,3S*)-2-methyl-2,3-diphenyloxirane With sec.-butyllithium in tetrahydrofuran; hexane; cyclohexane
T=0°C; 0.0166667 h;
2: methyl iodide in tetrahydrofuran; hexane; cyclohexane
0.166667 h;
参考文献
Nagaki, Aiichiro; Takizawa, Eiji; Yoshida, Jun-Ichi
Chemistry - A European Journal, 2010 , vol. 16, # 47 p. 14149 - 14158
反应条件
water; oxygen in dichloromethane
T=80°C; 3 h; regioselective reaction;
参考文献
Xu, Ze-Feng; Cai, Chen-Xin; Liu, Jin-Tao
Organic Letters, 2013 , vol. 15, # 9 p. 2096 - 2099