1,2-二(苯基)丙-1-酮合成路线 (共 138 条)
反应条件
1: NaH / tetrahydrofuran / 0.25 h / Ambient temperature 2: benzene / 72 h / Irradiation View Scheme
参考文献
Koppes, Margareth J. C. M.; Crabbendam, Astrid M.; Cerfontain, Hans
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 11 p. 676 - 683
反应条件
1.1: NaI; Et3N / acetonitrile / 60 °C 2.1: SO2Cl2 / CH2Cl2 / 1 h / -40 °C 2.2: 4.25 g / CH2Cl2 / -40 - 20 °C 3.1: NaBH4 / methanol / 4 h View Scheme
参考文献
Maciagiewicz; Dybowski; Skowronska
Tetrahedron, 2003 , vol. 59, # 32 p. 6057 - 6066
反应条件
tetrachloromethane; potassium hydroxide; 18-crown-6 ether 2 h; Heating;
参考文献
Abele; Rubina; Shymanska; Lukevics
Synthetic Communications, 1995 , vol. 25, # 9 p. 1371 - 1376
反应条件
zinc(II) chloride T=330°C; anschliessend Behandeln mit Wasser;
参考文献
Saleskaja
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1172,1176
Chem.Abstr., 1949 , p. 1753
反应条件
Pd2hpp4; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; oxygen in tetrahydrofuran T=6°C; P=760.051 Torr; 12 h; regioselective reaction;
参考文献
Chuang, Gary Jing; Wang, Weike; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 6 p. 1760 - 1762
反应条件
oxygen; pyridine; compound with copper (II)-nitrate in methanol T=55°C; 72 h; Mechanism;
参考文献
Sayre, L. M.; Jin, S.-J.
Journal of Organic Chemistry, 1984 , vol. 49, # 19 p. 3498 - 3503
反应条件
sodium ethanolate; isopentyl nitrite
参考文献
Ney
Chemische Berichte, 1888 , vol. 21, p. 2448
参考文献
Ney
Chemische Berichte, 1888 , vol. 21, p. 2448
反应条件
potassium carbonate T=200°C; 6.2 h; Title compound not separated from byproducts;
参考文献
Selva, Maurizio; Marques, Carlos Alberto; Tundo, Pietro
Gazzetta Chimica Italiana, 1993 , vol. 123, # 9 p. 515 - 518
反应条件
triphenyl-arsane; hydrogen; N-ethyl-N,N-diisopropylamine; [RhCl(cycloocta-1,5-diene)2]B(3,5-(CF3)2C6H3)4 in diethylene glycol dimethyl ether
T=65°C; P=760 Torr;
参考文献
Hong, Young-Taek; Barchuk, Andriy; Krische, Michael J.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 41 p. 6885 - 6888