(N,S-二甲基亚砜亚胺基)苯合成路线 (共 5 条)
反应条件
sodium azide; sulfuric acid in chloroform
参考文献
Hendriks, Christine M. M.; Lamers, Philip; Engel, Julien; Bolm, Carsten
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 17 p. 3363 - 3368
反应条件
1.1: dihydrogen peroxide / water / 40 °C 2.1: sodium azide; sulfuric acid / chloroform / Inert atmosphere 2.2: 12 h / 0 - 45 °C View Scheme
参考文献
Hendriks, Christine M. M.; Lamers, Philip; Engel, Julien; Bolm, Carsten
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 17 p. 3363 - 3368
反应条件
1.1: sodium hydroxide / ethanol / 0.5 h 1.2: 3 h / 20 °C 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 0 °C 3.1: tetrahydrofuran / 2 h / |Reflux 4.1: sodium periodate; RuCl3*4H2O / acetonitrile; water / 1 h / 20 °C 5.1: sulfuric acid / water / 2 h / 110 °C View Scheme
参考文献
Hendriks, Christine M. M.; Lamers, Philip; Engel, Julien; Bolm, Carsten
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 17 p. 3363 - 3368
参考文献
Oae,S. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 2856 - 2858
反应条件
tert.-butylnitrite in chloroform T=25°C; 0.25 h;
参考文献
Akutagawa, Kunihiko; Furukawa, Naomichi; Oae, Shigeru
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 369 - 374