1: enolate sodique de l'acetylacetate d'ethyle With n-butyllithium in tetrahydrofuran; hexane 0.333333 h; 2: (Z)-1-bromo-3,7-dimethyl-octa-2,6-diene in tetrahydrofuran; hexane T=0°C; 0.5 h; Further stages.;
参考文献
Shao, Ying; Eummer, Jeffrey T.; Gibbs, Richard A.
Organic Letters, 1999 , vol. 1, # 4 p. 627 - 630
tetrachloromethane in dimethyl sulfoxide 16 h; Heatingat 20 - 25 deg C in different bipolar aprotic solvents;
参考文献
Terpigorev, A. N.; Shcherbin, M. B.; Bazanov, A. G.; Tselinskii, I. V.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 2175 - 2178
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 12 p. 2545 - 2549
1: enolate sodique de l'acetylacetate d'ethyle With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2: 3-iodoprop-1-ene in tetrahydrofuran; hexane T=20°C; 1.5 h;
参考文献
Bargiggia, Frederic C.; Murray, William V.
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9636 - 9639
Mackay, Donald; Dao, Le H.; Dust, Julian M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2408 - 2416
1: enolate sodique de l'acetylacetate d'ethyle With n-butyllithium in tetrahydrofuran; cyclohexane
T=0°C; 0.5 h;
2: prenyl bromide in tetrahydrofuran; cyclohexane
0.5 h; Further stages.;
参考文献
Rawat, Diwan S; Gibbs, Richard A
Organic letters, 2002 , vol. 4, # 18 p. 3027 - 3030
