3-(4-甲氧基苯基)丙醛合成路线 （共 75 条）
反应条件
hydrogen; [Rh(cod)(π6-benzoic acid)]BF4 coated Co-ferrite 3 h; organic-soluble nanomagnet supported catalyst was reused several times; Kinetics; Further Variations:Catalysts;
参考文献
New Journal of Chemistry, , vol. 27, # 2 p. 227 - 229
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; 1,3-bis-(diphenylphosphino)propane; hydrogen in water; toluene T=120°C; P=7500.75 Torr; 20 h; Overall yield = 74 percentChromat.; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 54, # 18 p. 2209 - 2211
反应条件
triethylsilane; palladium on activated charcoal in acetone T=20°C; 0.666667 h;
参考文献
Miyazaki, Tohru; Han-Ya, Yuki; Tokuyama, Hidetoshi; Fukuyama, Tohru
Synlett, 2004 , # 3 p. 477 - 480
反应条件
1: With phenyl silane; triethylamine in tetrahydrofuran T=20°C; 2 h; Inert atmosphere; 2: With water 0.25 h; Inert atmosphere;
参考文献
Frost, Christopher G.; Hartley, Benjamin C.
Journal of Organic Chemistry, 2009 , vol. 74, # 9 p. 3599 - 3602
反应条件
hydrogen; [rhodium(acetylacetonate)(CO)2]; (tetra-tBu-biphenyl-2)phosphite-tbdps-2,5-anhydro-D-mannitol in toluene T=40°C; P=15001.5 Torr; 15 h; Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 11-12 p. 1983 - 1998
反应条件
1: With methyl-diethoxy-silane; Rh<(S,S)-Phebox-i-Pr>(OAc)2(aq) in toluene T=60°C; 2: With potassium fluoride; tetrabutyl ammonium fluoride in tetrahydrofuran; methanol; toluene Further stages.;
参考文献
Synlett, , # 19 p. 3343 - 3345
反应条件
tetrabutyl-ammonium chloride; sodium hydrogencarbonate; palladium diacetate in water T=80°C; 24 h;
参考文献
Zhao; Cai; Hu; Song
Synthetic Communications, 2001 , vol. 31, # 23 p. 3665 - 3669
反应条件
1.1: 72 percent / H2O / 2 h / 75 °C 2.1: N-methylmorpholine-N-oxide; PhSiH3 / Mo(CO)6 / tetrahydrofuran / 16 h / 80 °C 2.2: 85 percent / H2O / tetrahydrofuran / 0.25 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 9, # 21 p. 4259 - 4261
反应条件
oxygen; palladium diacetate; copper(l) chloride in dimethyl sulfoxide T=50°C; P=760.051 Torr; 20 h; regioselective reaction;
参考文献
Chen, Mao; Wang, Jie; Chai, Ziyi; You, Cai; Lei, Aiwen
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 341 - 346
反应条件
dimethylphenylsilane; C19H8O7Ru3 in 1,4-dioxane T=20°C; 1 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 15 p. 3243 - 3252
