1-(2-甲基苯基)丙-1-酮合成路线 (共 24 条)
反应条件
jones reagent in acetone T=20 - 30°C;
参考文献
Journal of Organic Chemistry, , vol. 51, # 9 p. 1402 - 1406
反应条件
1: ortho-methylbenzoic acid With oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane T=20°C; 0.333333 h; 2: ethyl magnesium chloride With iron (III) acetylacetonate in tetrahydrofuran T=20°C; 0.333333 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 28 p. 10028 - 10038
反应条件
1: ethyl iodide With iodine; magnesium in diethyl ether 1.5 h; Heating; 2: 2-methylbenzonitrile in diethyl ether Grignard reaction; 2 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 69, # 22 p. 7582 - 7591
反应条件
1: 92 percent / diethyl ether 2: 69 percent / CrO3; H2SO4 / acetone; H2O / 2 h / 10 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 4 p. 1594 - 1596
参考文献
Journal of the American Chemical Society, , vol. 75, p. 5899
反应条件
HZSM-5 T=250°C; 12 h; other catalyst: HY-Zeolite; Yield given;
参考文献
Synthetic Communications, , vol. 27, # 5 p. 777 - 780
参考文献
Journal of the American Chemical Society, , vol. 71, p. 1362,1366
Bulletin de la Societe Chimique de France, , vol. <5> 7, p. 527,669
反应条件
1: n-butyllithium 2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / Reflux View Scheme
参考文献
Chinese Journal of Chemistry, , vol. 30, # 6 p. 1289 - 1294
反应条件
Zersetzung des Reaktionsprodukts mit Wasser;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 133, p. 1218