2,4,5-三氟苯甲酸甲酯合成路线 （共 4 条）
反应条件
1: With diazomethyl-trimethyl-silane in hexane; toluene 0.0833333 h; 2: With acetic acid in hexane; toluene
参考文献
PROSIDION LIMITED
Patent: WO2007/3960 A1, 2007 ;
Location in patent: Page/Page column 32 ;
WO 2007/003960 A1
反应条件
1: (COCl)2 / dioxane / 0.5 h / Ambient temperature 2: tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Terauchi, Hideo; Tanitame, Akihiko; Tada, Keiko; Nishikawa, Yoshinori
Heterocycles, 1996 , vol. 43, # 8 p. 1719 - 1734
反应条件
in tetrahydrofuran 0.5 h; Ambient temperature; Yield given;
参考文献
Terauchi, Hideo; Tanitame, Akihiko; Tada, Keiko; Nishikawa, Yoshinori
Heterocycles, 1996 , vol. 43, # 8 p. 1719 - 1734
反应条件
sodium thiomethoxide in N,N-dimethyl-formamide
T=-78 - 20°C; 2.5 h;
参考文献
PROSIDION LIMITED
Patent: WO2007/3960 A1, 2007 ;
Location in patent: Page/Page column 32 ;
WO 2007/003960 A1
