1-氧代-2-甲基-6,7-二甲氧基-1,2-二氢异喹啉合成路线 （共 25 条）
反应条件
toluene-4-sulfonic acid in toluene
0.666667 h; Heating;
参考文献
Lee, Albert, W. M.; Chan, Wing Hong; Chan, Eddy T. T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 3 p. 309 - 310
反应条件
sodium methylsulfinylmethanide in dimethyl sulfoxide
T=40 - 45°C; 15 h;
参考文献
Lera, Angel Rodriguez de; Aubourg, Santiago; Suau, Rafael; Castedo, Luis
Heterocycles, 1987 , vol. 26, # 3 p. 675 - 684
反应条件
1: DCC / CH2Cl2
2: 84 percent / 6.5 h / Heating
3: 93 percent / toluene-p-sulfonic acid monohydrate / toluene / 0.67 h / Heating
View Scheme
参考文献
Lee, Albert, W. M.; Chan, Wing Hong; Chan, Eddy T. T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 3 p. 309 - 310
反应条件
1: 84 percent / 6.5 h / Heating
2: 93 percent / toluene-p-sulfonic acid monohydrate / toluene / 0.67 h / Heating
View Scheme
参考文献
Lee, Albert, W. M.; Chan, Wing Hong; Chan, Eddy T. T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 3 p. 309 - 310
参考文献
Lee, Albert, W. M.; Chan, Wing Hong; Chan, Eddy T. T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 3 p. 309 - 310
反应条件
methanamine monoacetate in methanol
T=100°C; fragmentation;
参考文献
Lapa; Tolkachev
Pharmaceutical Chemistry Journal, 1999 , vol. 33, # 7 p. 377 - 378
反应条件
methanamine monoacetate in methanol
T=100°C; fragmentation; 72 h;
参考文献
Lapa; Tolkachev
Pharmaceutical Chemistry Journal, 1999 , vol. 33, # 7 p. 377 - 378
反应条件
trichloroacetic acid in benzene
0.7 h; Heating;
参考文献
Lee, Albert, W. M.; Chan, Wing Hong; Chan, Eddy T. T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 3 p. 309 - 310
反应条件
Fremy’s salt; anhydrous carbonate in ethanol; water
72 h; Mechanism;
参考文献
Castedo, Luis; Puga, Alberto; Saa, Jose M.; Suau, Rafael
Tetrahedron Letters, 1981 , vol. 22, # 23 p. 2233 - 2236
反应条件
1: acetonitrile / 2 h / 80 °C
2: 1) AgCl, 2) rat liver enzymes / 1) methanol, 2) 37 deg C, 2 h, pH 7.5
View Scheme
参考文献
Walterova; Preininger; Dolejs; et al.
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 3 p. 956 - 965
