2-苯甲酰基-1-苯并呋喃-3(2H)-酮合成路线 (共 10 条)
反应条件
1: 63 mg / tri-n-butyltin hydride / benzene / 0.5 h / Heating; further reagents 2: 99 mg / N-bromosuccinimide / acetic acid; acetic anhydride / 1 h 3: 59 mg / aq. sodium hydroxide / dioxane / 1.25 h View Scheme
参考文献
Bird, T. Geoffrey C.; Brown, Ben R.; Stuart, Ian A.; Tyrrell, William R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1831 - 1846
反应条件
potassium hydroxide in ethanol 2 h; Heating;
参考文献
Sahasrabhuddhe; Ghiya
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 61 - 63
反应条件
potassium hydroxide in 1,4-dioxane 0.5 h; Heating;
参考文献
Joshi, M. G.; Wadokar, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 10 p. 930 - 931
反应条件
1: 85 percent / acetonitrile; dioxane; tetrahydrofuran / 2 h / Heating 2: KOH / dioxane / 0.5 h / Heating View Scheme
参考文献
Joshi, M. G.; Wadokar, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 10 p. 930 - 931
反应条件
lithium hexamethyldisilazane in toluene T=20°C; 0.166667 h;
参考文献
Atobe, Masakazu; Naganuma, Kenji; Kawanishi, Masashi; Morimoto, Akifumi; Kasahara, Ken-Ichi; Ohashi, Shigeki; Suzuki, Hiroko; Hayashi, Takahiko; Miyoshi, Shiro
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 24 p. 6569 - 6576
反应条件
potassium hydroxide in 1,4-dioxane 0.5 h; Heating; Yield given;
参考文献
Prakash; Goyal
Synthesis, 1992 , # 7 p. 629 - 630
反应条件
1: 80 percent / copper(II) chloride-DMSO / 2 h / Heating 2: 60 percent / 10percent KOH / ethanol / 2 h / Heating View Scheme
参考文献
Sahasrabhuddhe; Ghiya
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 61 - 63
反应条件
sodium hydroxide in 1,4-dioxane 1.25 h;
参考文献
Bird, T. Geoffrey C.; Brown, Ben R.; Stuart, Ian A.; Tyrrell, William R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1831 - 1846
反应条件
sodium hydroxide 1 h; Heating;
参考文献
Sonare, S. S.; Doshi, A. G.
Journal of the Indian Chemical Society, 1992 , vol. 69, # 12 p. 875
反应条件
acetic acid; hydrazine
参考文献
Mosher,W.A. et al.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2402 - 2405