2-(1-甲基-2-氧代丙基)-1H-异吲哚-1,3-(2H)-二酮合成路线 (共 5 条)
反应条件
bis(benzonitrile)palladium(II) dichloride; AgNO2; CuCl2·2H2O; nitromethane; oxygen; tert-butyl alcohol T=20°C; Wacker Oxidation; P=760.051 Torr; 6 h;
参考文献
Wickens, Zachary K.; Morandi, Bill; Grubbs, Robert H.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 43 p. 11257 - 11260
Angew. Chem., 2013 , vol. 125, # 43 p. 11467 - 11470
反应条件
T=20°C; 0.233333 h; Ionic liquid;
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal A.; Mukherjee, Debaraj; Taneja, Subhash C.
Synthetic Communications, 2013 , vol. 43, # 4 p. 505 - 519
反应条件
in N,N-dimethyl-formamide T=20°C;
参考文献
Yang, Ya Jun; Yang, Ya Nan; Jiang, Jian Shuang; Feng, Zi Ming; Liu, Hong Yan; Pan, Xian Dao; Zhang, Pei Cheng
Chinese Chemical Letters, 2010 , vol. 21, # 8 p. 902 - 904
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide T=60°C; 17 h;
参考文献
Hoye, Thomas R.; Duff, Steven R.; King, Rita S.
Tetrahedron Letters, 1985 , vol. 26, # 29 p. 3433 - 3436
反应条件
1: pyridine / CH2Cl2 2: 1.8 g / pyridine / acetic acid; H2O View Scheme
参考文献
Zav'yalov, S. I.; Ezhova, G. I.; Budkova, T. K.; Dorofeeva, O. V.; Taganova, O. K.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 2 p. 424 - 427
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 2 p. 468 - 471