4-(3,4-二甲氧基苯基)-1,2-二甲氧基苯合成路线 （共 30 条）
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran
T=20°C; 40 h; Inert atmosphere;
参考文献
Kianmehr, Ebrahim; Rajabi, Azam; Ghanbari, Mohammad
Tetrahedron Letters, 2009 , vol. 50, # 15 p. 1687 - 1688
反应条件
sodium methylate; copper(I) bromide in water; N,N-dimethyl-formamide
2 h; Heating;
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
反应条件
pyridine in chloroform
T=60°C;
参考文献
Combes; Finet; Siri
Journal of the Chemical Society. Perkin Transactions 1, 2002 , vol. 2, # 1 p. 38 - 44
反应条件
4-iodoveratrole; copper
T=235 - 280°C;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
1: 83 percent / H2SO4; dimethyldioxirane; NaBr / acetone
2: 70 percent / sodium methylate; CuBr / dimethylformamide; H2O / 2 h / Heating
View Scheme
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
反应条件
1: 1.7 M t-butyl lithium / tetrahydrofuran; pentane / 0.5 h / 0 °C
2: 1.) Te; 2.) O2 / 1.) THF, pentane, room temperature, 5 h; 2.) 1 h
View Scheme
参考文献
Engman, Lars
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 413 - 416
反应条件
3,4-dimethyliodobenzene; copper
T=235 - 280°C;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
1: SeCl4 / tetrahydrofuran; pentane / 2 h / Ambient temperature
2: 10percent aq. Na2S2O5 / CH2Cl2
View Scheme
参考文献
Engman, Lars
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 413 - 416
反应条件
copper
T=235 - 280°C;
参考文献
Bushby, Richard J.; Hardy, Cristopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 721 - 724
反应条件
Na2S2O5 in dichloromethane
Yield given;
参考文献
Engman, Lars
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 413 - 416
