4-(3,4-二甲氧基苯基)-1,2-二甲氧基苯合成路线 (共 30 条)
反应条件
boron tribromide in dichloromethane 1 h;
参考文献
Joulie, Laurent F.; Schatz, Erik; Ward, Michael D.; Weber, Frank; Yellowlees, Lesley J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1994 , # 6 p. 799 - 804
反应条件
tetra-n-butylammonium tetrafluoroborate in dichloromethane; trifluoroacetic acid T=12°C; electrolysis;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 36, # 5 p. 317 - 326
反应条件
sodium carbonate; palladium dichloride in ethanol; water
T=150°C; Suzuki-Miyaura Coupling; 0.166667 h; Microwave irradiation;
参考文献
Stevens, Craig B.; Hanna Jr., James M.; Lammi, Robin K.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 6 p. 1703 - 1706
反应条件
1: 1-iodo-n-undecane With [Fe(C2H4)4][Li(tmeda)]2 in tetrahydrofuran
T=-20°C;
2: 4-(magnesium halide)-1,2-dimethoxybenzene in tetrahydrofuran; diethyl ether
T=-20°C; Further stages.;
参考文献
Fuerstner, Alois; Martin, Ruben; Krause, Helga; Seidel, Guenter; Goddard, Richard; Lehmann, Christian W.
Journal of the American Chemical Society, 2008 , vol. 130, # 27 p. 8773 - 8787
反应条件
[2,2']bipyridinyl; nickel diacetate; lithium tert-butylate in tetrahydrofuran
T=63°C; Homocoupling; 74 h;
参考文献
Massicot, Fabien; Schneider, Raphael; Fort, Yves
Journal of Chemical Research - Part S, 1999 , # 11 p. 664 - 665
反应条件
copper
T=260 - 280°C; 2 h;
参考文献
Yamato, Takehiko; Hideshima, Chieko; Suehiro, Kazuaki; Tashiro, Masashi; Prakash, G. K. Surya; Olah, George A.
Journal of Organic Chemistry, 1991 , vol. 56, # 21 p. 6248 - 6250
反应条件
copper(l) chloride in methanol
T=25°C; 3 h;
参考文献
Cheng, Guanjun; Luo, Meiming
European Journal of Organic Chemistry, 2011 , # 13 p. 2519 - 2523
反应条件
palladium diacetate; copper dichloride in tetrahydrofuran
T=23°C; 0.5 h;
参考文献
Parrish, Jay P.; Flanders, Vincent L.; Floyd, Ryan J.; Jung, Kyung Woon
Tetrahedron Letters, 2001 , vol. 42, # 44 p. 7729 - 7731
反应条件
magnesium; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran
T=20°C;
参考文献
Vagin, Sergei; Hanack, Michael
European Journal of Organic Chemistry, 2003 , # 14 p. 2661 - 2669
反应条件
4-nitropyrazole; tetrabutylammonium salt of 4-nitropyrazole in acetonitrile
Electrochemical reaction;
参考文献
Petrosyan; Burasov
Russian Chemical Bulletin, 2010 , vol. 59, # 3 p. 522 - 527