5-(3-氨基丙基)-1H-咪唑-2-胺合成路线 (共 5 条)
反应条件
sodium hydroxide 8 h; Heating;
参考文献
Foley,L.H.; Buechi,G.
Journal of the American Chemical Society, 1982 , vol. 104, p. 1776
反应条件
triethylamine in ethanol
参考文献
Shengule, Sudhir R.; Karuso, Peter
Australian Journal of Chemistry, 2014 , vol. 67, # 2 p. 184 - 191
参考文献
Olofson, Anne; Yakushijin, Kenichi; Horne, David A.
Journal of Organic Chemistry, 1997 , vol. 62, # 23 p. 7918 - 7919
反应条件
1.1: thionyl chloride / 8 h / 0 °C / |Reflux 2.1: hydrogenchloride; sodium amalgam / water / 0 °C / pH 1 - 3 2.2: 2 h / 95 °C / pH 4.5 3.1: triethylamine / ethanol View Scheme
参考文献
Australian Journal of Chemistry, , vol. 67, # 2 p. 184 - 191
反应条件
1.1: hydrogenchloride; sodium amalgam / water / 0 °C / pH 1 - 3 1.2: 2 h / 95 °C / pH 4.5 2.1: triethylamine / ethanol View Scheme
参考文献
Australian Journal of Chemistry, , vol. 67, # 2 p. 184 - 191