6-甲氧基-2,2-二甲基-3,4-二氢-2H-苯并[h]色烯合成路线 （共 10 条）
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate Catalytic hydrogenation; P=2068.59 Torr; 1 h;
参考文献
Alves, Glaucia B. C.; Lopes, Rosangela S. C.; Lopes, Claudio C.; Snieckus, Victor
Synthesis, 1999 , # 11 p. 1875 - 1877
反应条件
3,4,5,6-tetrachloro-1,2-benzoquinone; [Mo(CO)3(cyclopentadienyl)Cl] in chlorobenzene T=150°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Yamamoto, Yoshihiko; Itonaga, Kouhei
Organic Letters, 2009 , vol. 11, # 3 p. 717 - 720
反应条件
1: 98 percent / phenylboronic acid / acetic acid; toluene / 4 h / Heating 2: 100 percent / H2 / 10 percent Pd/C / ethyl acetate / 1 h / 2068.59 Torr View Scheme
参考文献
Wang, Xue; Chen, Ye; Lee, Yong Rok
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 153 - 156
反应条件
1: 98 percent / phenylboronic acid / acetic acid; toluene / 4 h / Heating 2: 100 percent / H2 / 10 percent Pd/C / ethyl acetate / 1 h / 2068.59 Torr View Scheme
参考文献
Wang, Xue; Chen, Ye; Lee, Yong Rok
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 153 - 156
反应条件
hydrogenchloride; mercury dichloride; zinc 3 h; Heating;
参考文献
Paradkar, Madhusudan V.; Godbole, Himanshu M.; Ranade, Anup A.; Joseph, Augustine R.
Journal of Chemical Research - Part S, 1998 , # 6 p. 318 - 319
反应条件
1: 60 percent / pyrrolidine / benzene / 48 h / Heating 2: 78 percent / Zn, HgCl2, aq. HCl / 3 h / Heating View Scheme
参考文献
Paradkar, Madhusudan V.; Godbole, Himanshu M.; Ranade, Anup A.; Joseph, Augustine R.
Journal of Chemical Research - Part S, 1998 , # 6 p. 318 - 319
反应条件
zinc(II) chloride; benzene
参考文献
Livingstone; Whiting
Journal of the Chemical Society, 1955 , p. 3631,3635
反应条件
ammonium cerium(IV) nitrate; water in acetonitrile T=0 - 5°C; Oxidation; 0.5 h;
参考文献
Alves, Glaucia B. C.; Lopes, Rosangela S. C.; Lopes, Claudio C.; Snieckus, Victor
Synthesis, 1999 , # 11 p. 1875 - 1877
反应条件
ammonium cerium (IV) nitrate in ethylene glycol dimethyl ether; water T=20°C; 8 h; Inert atmosphere;
参考文献
Wang, Xue; Chen, Ye; Lee, Yong Rok
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 153 - 156
反应条件
ammonium cerium (IV) nitrate in ethylene glycol dimethyl ether; water
T=20°C; 8 h; Inert atmosphere;
参考文献
Wang, Xue; Chen, Ye; Lee, Yong Rok
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 153 - 156
