3-(2-噻吩基)-DL-丙氨酸合成路线 （共 26 条）
反应条件
lithium hydroxide T=60°C; 2.5 h;
参考文献
Chemistry - A European Journal, , vol. 12, # 10 p. 2739 - 2744
反应条件
barium dihydroxide; water Erwaermen des erhaltenen Barium-Salzes mit wss. Schwefelsaeure;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 14, p. 263
反应条件
1.1: NaBH4 / methanol / 20 °C 2.1: SOCl2; benzotriazole / CH2Cl2 3.1: NaH / dimethylformamide; various solvent(s) / 0.5 h / 20 °C 3.2: 82 percent / dimethylformamide; various solvent(s) / 7 h / 20 - 60 °C 4.1: NaOH / methanol / 20 h / 20 °C 5.1: toluene / 2 h / Heating 6.1: 75 percent / aq. LiOH / 2.5 h / 60 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 12, # 10 p. 2739 - 2744
反应条件
ammonium hydroxide; hydrogen sulfide Erhitzen des Reaktionsgemisches auf 100grad;
参考文献
Journal of Biological Chemistry, , vol. 159, p. 385,392
反应条件
1.1: NaH / dimethylformamide; various solvent(s) / 0.5 h / 20 °C 1.2: 82 percent / dimethylformamide; various solvent(s) / 7 h / 20 - 60 °C 2.1: NaOH / methanol / 20 h / 20 °C 3.1: toluene / 2 h / Heating 4.1: 75 percent / aq. LiOH / 2.5 h / 60 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 12, # 10 p. 2739 - 2744
反应条件
1: toluene / 2 h / Heating 2: 75 percent / aq. LiOH / 2.5 h / 60 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 12, # 10 p. 2739 - 2744
反应条件
1.1: SOCl2; benzotriazole / CH2Cl2 2.1: NaH / dimethylformamide; various solvent(s) / 0.5 h / 20 °C 2.2: 82 percent / dimethylformamide; various solvent(s) / 7 h / 20 - 60 °C 3.1: NaOH / methanol / 20 h / 20 °C 4.1: toluene / 2 h / Heating 5.1: 75 percent / aq. LiOH / 2.5 h / 60 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 12, # 10 p. 2739 - 2744
反应条件
sodium amalgam; ethanol
参考文献
Journal of Organic Chemistry, , vol. 15, p. 81,87
参考文献
Journal of Biological Chemistry, , vol. 166, p. 541
Journal of the American Chemical Society, , vol. 71, p. 1201,1202
反应条件
1: ethanol; hydroxylamine 2: ethanol; sodium-amalgam View Scheme
参考文献
Journal of Organic Chemistry, , vol. 15, p. 81,87
