反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '605461', constants.ctx, '0')">phenylacetylene</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209227', constants.ctx, '0')">n-butyllithium</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78°C; 0.5 h; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '1209486', constants.ctx, '0')">glyoxylic acid ethyl ester</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a>; <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=-78°C; 6 h; <br />
参考文献
Felfer, Ulfried; Goriup, Marian; Koegl, Marion F.; Wagner, Ulrike; Larissegger-Schnell, Barbara; Faber, Kurt; Kroutil, Wolfgang Advanced Synthesis and Catalysis, 2005 , vol. 347, # 7-8 p. 951 - 961