3-甲基-2-氧代丁酰乙酯合成路线 （共 59 条）
参考文献
Mitani, Michiharu; Tanaka, Yasunori; Sawada, Akihiko; Misu, Ayuko; Matsumoto, Yoshihiro
European Journal of Organic Chemistry, 2008 , # 8 p. 1383 - 1391
反应条件
zinc(II) chloride in diethyl ether 23 h; Ambient temperature;
参考文献
Akiyama, Yasunobu; Kawasaki, Tomomi; Sakamoto, Masanori
Chemistry Letters, 1983 , p. 1231 - 1232
反应条件
1: hydrogen / 5 percent Pd/C / ethanol / 2585.7 Torr 2: Jones reagent / acetone / 0.5 h / Ambient temperature View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 61, p. 1397 - 1404
反应条件
nitrosyl sulfuric acid
参考文献
Chemische Berichte, , vol. 75, p. 121
反应条件
1: sodium azide / dimethylformamide / 2.5 h / 25 °C 2: 94 percent Chromat. / ethanol, n-butyllithium / 1) hexane, THF, 25 deg C, 2) 30 min, 25 deg C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 24 p. 4952 - 4954
反应条件
1: isopropyl bromide With magnesium in tetrahydrofuran T=20°C; 1 h; 2: oxalic acid diethyl ester in tetrahydrofuran T=-78 - -10°C; 1 h;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 10 p. 2658 - 2661
Angew. Chem., , vol. 126, # 10 p. 2696 - 2699,4
参考文献
Tetrahedron Letters, , vol. 26, # 35 p. 4261 - 4264
反应条件
1: N-chlorosuccinimide / CCl4 / 2 h / Heating 2: 66 percent / Hg(OAc)2 / acetone; H2O / 1 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 56, # 38 p. 7495 - 7502
反应条件
1: tert-butyl hypochlorite / diethyl ether / 0.5 h / 0 °C 2: sodium ethoxide / ethanol / 1 h / 40 °C 3: 5percent sulfuric acid / H2O / 2 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 3 p. 887 - 894
反应条件
1: tert-butyl hypochlorite / diethyl ether / 0.5 h / 0 °C 2: sodium ethoxide / ethanol / 1 h / 40 °C 3: 5percent sulfuric acid / H2O / 2 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 3 p. 887 - 894
