1,3,3-三甲基-2,3-二氢-1H-吲哚-2-酮合成路线 （共 67 条）
反应条件
1: With dibenzoyl peroxide in dichloromethane T=80°C; 18 h; 2: With sodium hydroxide in methanol T=20°C; 18 h; 3: With ammonia in methanol T=20°C; 4 h; Further stages.;
参考文献
Van Henegouwen; Fieseler; Rutjes; Hiemstra
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8317 - 8325
反应条件
copper(I) oxide; 1,2-diamino-benzene; sodium t-butanolate in tert-butyl alcohol
T=100°C; 48 h; Sealed tube;
参考文献
Jhan, Yu-Huei; Kang, Ting-Wei; Hsieh, Jen-Chieh
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1155 - 1159
反应条件
palladium diacetate; sodium t-butanolate; tri-cyclo-hexyl-phosphine in 1,4-dioxane
T=70°C; 3 h;
参考文献
Lee; Hartwig
Journal of Organic Chemistry, 2001 , vol. 66, # 10 p. 3402 - 3415
反应条件
sodium hydride in tetrahydrofuran
T=20°C; 18 h;
参考文献
Van Henegouwen; Fieseler; Rutjes; Hiemstra
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8317 - 8325
反应条件
trichlorophosphate in 1,4-dioxane
T=80°C; 4 h; Yields of byproduct given;
参考文献
Prizhiyalgovskaya, N. M.; Kon'kov, L. I.; Tarshits, D. L.; Salmina, S. V.; Segizova, N. T.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 7 p. 751 - 754
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 7 p. 915 - 918
反应条件
trichlorophosphate in 1,4-dioxane
T=80°C; 4 h; Yields of byproduct given;
参考文献
Prizhiyalgovskaya, N. M.; Kon'kov, L. I.; Tarshits, D. L.; Salmina, S. V.; Segizova, N. T.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 7 p. 751 - 754
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 7 p. 915 - 918
反应条件
trichlorophosphate in 1,4-dioxane
T=80°C; 4 h; Yields of byproduct given;
参考文献
Prizhiyalgovskaya, N. M.; Kon'kov, L. I.; Tarshits, D. L.; Salmina, S. V.; Segizova, N. T.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 7 p. 751 - 754
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 7 p. 915 - 918
反应条件
trichlorophosphate in 1,4-dioxane
T=85°C; 7 h;
参考文献
Tarshits, D. L.; Przhiyalgovskaya, N. M.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , vol. 24, # 11 p. 1217 - 1221
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , vol. 24, # 11 p. 1472 - 1475
反应条件
in tert-butyl alcohol
T=80°C; 2 h;
参考文献
Leroi, Corinne; Bertin, Denis; Dufils, Pierre-Emmanuel; Gigmes, Didier; Marque, Sylvain; Tordo, Paul; Couturier, Jean-Luc; Guerret, Olivier; Ciufolini, Marco A.
Organic Letters, 2003 , vol. 5, # 26 p. 4943 - 4945
反应条件
triethyl borane; tert.-butyl lithium; tert-butyl N-indolecarboxylate; palladium diacetate; triphenylphosphine in tetrahydrofuran
6 h; Heating;
参考文献
Ishikura, Minoru; Takahashi, Norinobu; Yamada, Koji; Yanada, Reiko
Tetrahedron, 2006 , vol. 62, # 50 p. 11580 - 11591
