Aceanthrylene合成路线 （共 16 条）
反应条件
ammonia; sodium in tetrahydrofuran T=-78°C; 0.5 h;
参考文献
Rabideau, Peter W.; Mooney, Jennifer L.; Smith, W. Kimmer; Sygula, Andrzej; Paschal, Jonathan W.
Journal of Organic Chemistry, 1988 , vol. 53, # 3 p. 589 - 591
反应条件
T=1100°C; 0.000555556 h; Product distributionMechanism;
参考文献
Journal of the American Chemical Society, , vol. 109, # 18 p. 5461 - 5465
反应条件
aluminum oxide in toluene
0.166667 h; Heating;
参考文献
Cohen, Yoram; Roelofs, Nicolas H.; Reinhardt, Gerd; Scott, Lawrence T.; Rabinovitz, Mordecai
Journal of Organic Chemistry, 1987 , vol. 52, # 19 p. 4207 - 4214
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene
1.5 h; Heating;
参考文献
Boerrigter, Jos C. Olde; Mulder, Patrick P. J.; Gen, Arne van der; Mohn, Georges R.; Cornelisse, Jan; Lugtenburg, Johan
Recueil des Travaux Chimiques des Pays-Bas, 1989 , vol. 108, # 2 p. 79 - 80
反应条件
toluene-4-sulfonic acid in toluene
1.25 h; Heating;
参考文献
Becker, Hans-Dieter; Hansen, Lars; Andersson, Kjell
Journal of Organic Chemistry, 1985 , vol. 50, # 2 p. 277 - 279
反应条件
1: 1.) hydrazine hydrate, 2.) KOH / 1.) diethylene glycol, reflux, 2.) diethylene glycol, 195 deg C, 3 h
2: 76 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / toluene / Heating
View Scheme
参考文献
Boerrigter, Jos C. Olde; Mulder, Patrick P. J.; Gen, Arne van der; Mohn, Georges R.; Cornelisse, Jan; Lugtenburg, Johan
Recueil des Travaux Chimiques des Pays-Bas, 1989 , vol. 108, # 2 p. 79 - 80
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
0.5 h; Heating;
参考文献
Chung, Ying-Sheng; Kruk, Henry; Barizo, Ophelia M.; Katz, Morris; Lee-Ruff, Edward
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1284 - 1288
反应条件
1: 56 percent / Br2 / diethyl ether / 5 h
2: 60 percent / AlCl3 / CS2 / 2 h
3: 95 percent / NaBH4 / tetrahydrofuran; methanol / 2 h / Ambient temperature
4: 93 percent / Al2O3 / toluene / 0.17 h / Heating
View Scheme
参考文献
Cohen, Yoram; Roelofs, Nicolas H.; Reinhardt, Gerd; Scott, Lawrence T.; Rabinovitz, Mordecai
Journal of Organic Chemistry, 1987 , vol. 52, # 19 p. 4207 - 4214
反应条件
1: 60 percent / AlCl3 / CS2 / 2 h
2: 95 percent / NaBH4 / tetrahydrofuran; methanol / 2 h / Ambient temperature
3: 93 percent / Al2O3 / toluene / 0.17 h / Heating
View Scheme
参考文献
Cohen, Yoram; Roelofs, Nicolas H.; Reinhardt, Gerd; Scott, Lawrence T.; Rabinovitz, Mordecai
Journal of Organic Chemistry, 1987 , vol. 52, # 19 p. 4207 - 4214
反应条件
1: 95 percent / NaBH4 / tetrahydrofuran; methanol / 2 h / Ambient temperature
2: 93 percent / Al2O3 / toluene / 0.17 h / Heating
View Scheme
参考文献
Cohen, Yoram; Roelofs, Nicolas H.; Reinhardt, Gerd; Scott, Lawrence T.; Rabinovitz, Mordecai
Journal of Organic Chemistry, 1987 , vol. 52, # 19 p. 4207 - 4214
