二[(对甲苯基)甲基]二硫醚合成路线 （共 10 条）
反应条件
1: 82 percent / N-bromosuccinimide / CH2Cl2 2: 10 percent / 0 deg C, 2.5 h -> 18 deg C, 2 h View Scheme
参考文献
Baudin, Jean-Bernard; Commenil, Marie-Gabrielle; Julia, Sylvestre A.; Lome, Robert; Ruel, Odile
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 11 p. 1127 - 1141
反应条件
1: 78 percent / N-bromosuccinimide / CH2Cl2 2: 3 percent Spectr. / LiOCH3 / tetrahydrofuran / 0 deg C, 15 min then 18 deg C, 1 h View Scheme
参考文献
Baudin, Jean-Bernard; Commenil, Marie-Gabrielle; Julia, Sylvestre A.; Lome, Robert; Ruel, Odile
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 11 p. 1127 - 1141
反应条件
Erhitzen unter Normaldruck;
参考文献
Bulmer; Mann
Journal of the Chemical Society, 1945 , p. 666,671
反应条件
1: 82 percent / N-bromosuccinimide / CH2Cl2 2: 29 percent Spectr. / LiOCH3 / methanol / 0 deg C, 15 min, 18 deg C, 2 h View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 11 p. 1127 - 1141
反应条件
1: 82 percent / N-bromosuccinimide / CH2Cl2 2: 7 percent / sodium methoxide / tetrahydrofuran / 4.5 h / 0 °C View Scheme
参考文献
Baudin, Jean-Bernard; Commenil, Marie-Gabrielle; Julia, Sylvestre A.; Lome, Robert; Ruel, Odile
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 11 p. 1127 - 1141
反应条件
1: bis-lt;(4-methylphenyl)methylgt;disulfide With tert-butylhypochlorite; water in acetonitrile T=0°C; 0.25 h; 2: benzylamine in acetonitrile T=0 - 20°C; 0.666667 h;
参考文献
Joyard, Yoann; Papamicael, Cyril; Bohn, Pierre; Bischoff, Laurent
Organic Letters, 2013 , vol. 15, # 9 p. 2294 - 2297
反应条件
di-tert-butyl peroxide; dicobalt octacarbonyl in benzene T=185°C; P=44080 Torr; in N2-atm.;
参考文献
Antebi, Shlomo; Alper, Howard
Tetrahedron Letters, 1985 , vol. 26, # 22 p. 2609 - 2612
反应条件
dicobalt octacarbonyl in benzene T=185°C; P=44080 Torr; in CO-atm.;
参考文献
Antebi, Shlomo; Alper, Howard
Tetrahedron Letters, 1985 , vol. 26, # 22 p. 2609 - 2612
反应条件
1: 82 percent / N-bromosuccinimide / CH2Cl2 2: 50 percent / 0 deg C, 2.5 h -> 18 deg C, 2 h View Scheme
参考文献
Baudin, Jean-Bernard; Commenil, Marie-Gabrielle; Julia, Sylvestre A.; Lome, Robert; Ruel, Odile
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 11 p. 1127 - 1141
反应条件
1: 78 percent / N-bromosuccinimide / CH2Cl2 2: 69 percent / LiOCH3 / tetrahydrofuran / 0 deg C, 15 min then 18 deg C, 1 h View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 11 p. 1127 - 1141
