9-(碘甲基)-9H-氧杂蒽合成路线 （共 3 条）
反应条件
1H-imidazole; triphenylphosphine diiodide in dichloromethane Ambient temperature;
参考文献
Ornstein, Paul L.; Bleisch, Thomas J.; Arnold, M. Brian; Wright, Rebecca A.; Johnson, Bryan G.; Schoepp, Darryle D.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 3 p. 346 - 357
反应条件
1: 10.0 M borane methyl sulfide / tetrahydrofuran / 0 - 20 °C 2: triphenylphosphine diiodide, imidazole / CH2Cl2 / Ambient temperature View Scheme
参考文献
Ornstein, Paul L.; Bleisch, Thomas J.; Arnold, M. Brian; Wright, Rebecca A.; Johnson, Bryan G.; Schoepp, Darryle D.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 3 p. 346 - 357
反应条件
tetrakis(triphenylphosphine) palladium(0); zinc copper 1.) benzene, N,N-dimethylacetamide, 60 deg C, 3 h, 2.) benzene, N,N-dimethylacetamide, RT, 1 h; Yield given. Multistep reaction;
参考文献
Ornstein, Paul L.; Bleisch, Thomas J.; Arnold, M. Brian; Kennedy, Joseph H.; Wright, Rebecca A.; Johnson, Bryan G.; Tizzano, Joseph P.; Helton, David R.; Kallman, Mary Jeanne; Schoepp, Darryle D.; Herin, Marc
Journal of Medicinal Chemistry, 1998 , vol. 41, # 3 p. 358 - 378
