N-苄氧羰基-L-亮氨酸合成路线 (共 125 条)
反应条件
1: 89 percent / quinoline; CH2Cl2 / 12 h / Ambient temperature 2: triethylamine; dioxane; H2O / 24 h / 22 °C View Scheme
参考文献
Chemische Berichte, , vol. 118, # 2 p. 468 - 482
反应条件
1: 1) NaH / 1) THF, reflux, 2h, 2) room temperature, 1h 2: tetrahydrofuran / 3 h / Ambient temperature 3: 72 percent / standard pH stat conditions View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 44 p. 5375 - 5376
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide; N-decanoyl-L-histidine methyl ester in water T=25°C; pH=7.30; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 5 - 10
反应条件
lithium hydroxide in tetrahydrofuran 1 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 24 p. 3584 - 3587
反应条件
1: 76 percent / CuI; Zn / aq. ethanol / sonification 2: aq. LiOH / tetrahydrofuran / 1 h View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 24 p. 3584 - 3587
反应条件
1: 52 percent / Et3N / CH2Cl2 / 4 h / 0 °C 2: Jones' reagent / acetone / 3 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 535 - 540
反应条件
1: triethylamine 2: lithium hydroxide hydrate; water / tetrahydrofuran View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 1 p. 62 - 65
反应条件
1: triethylamine / dichloromethane / 2.08 h / 0 - 20 °C 2: / dichloromethane / 1.08 h / 0 - 20 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 65, p. 436 - 447
反应条件
standard pH stat conditions;
参考文献
Sennyey, Gerard; Barcelo, Gerard; Senet, Jean-Pierre
Tetrahedron Letters, 1986 , vol. 27, # 44 p. 5375 - 5376
反应条件
in 1,4-dioxane; water; triethylamine T=22°C; 24 h; Yield given;
参考文献
Chemische Berichte, , vol. 118, # 2 p. 468 - 482