4-氰基-4-(硫代苯甲酰)戊酸合成路线 （共 11 条）
反应条件
in ethyl acetate T=85°C; 12 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 38 p. 10656 - 10658
反应条件
pyrrol-N-thiocarbonyl disulfides in ethyl acetate 20 h;
参考文献
US2004/138492 A1, ;
Page 4 ;
反应条件
in methanol T=80°C; 3 h;
参考文献
Chemical Communications, , # 19 p. 2230 - 2232
反应条件
1: m-dithiobenzoic acid With iodine; dimethyl sulfoxide in ethyl acetate 10 h; 2: V-501 in ethyl acetate 18 h; Heating;
参考文献
Macromolecules, , vol. 38, # 16 p. 6841 - 6848
反应条件
1: potassium ferricyanide / H2O / 1 h / 20 °C 2: ethyl acetate / 28.5 h / 70 °C View Scheme
参考文献
Macromolecules, , vol. 37, # 20 p. 7530 - 7537
反应条件
1: sulfur; MeONa / methanol / 10 h / 70 °C 2: potassium ferricyanide / H2O / 1 h / 20 °C 3: ethyl acetate / 28.5 h / 70 °C View Scheme
参考文献
Macromolecules, , vol. 37, # 20 p. 7530 - 7537
反应条件
1: iodine; dimethyl sulfoxide / ethanol / 2 h / 20 °C 2: ethyl acetate / 20 h / 80 °C / Inert atmosphere View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 89, # 3 p. 317 - 325
反应条件
in ethyl acetate T=80°C; 20 h; Inert atmosphere;
参考文献
Canadian Journal of Chemistry, , vol. 89, # 3 p. 317 - 325
反应条件
in ethyl acetate T=20°C; 28 h; Reflux;
参考文献
Chemistry - An Asian Journal, , vol. 9, # 1 p. 199 - 205
反应条件
1.1: iodine; magnesium / tetrahydrofuran / 1 h 1.2: 2 h / 0 °C 2.1: iodine; dimethyl sulfoxide / ethanol / 2 h / 20 °C 3.1: ethyl acetate / 20 h / 80 °C / Inert atmosphere View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 89, # 3 p. 317 - 325
