2-氰丙基-2-基苯并二硫合成路线 （共 14 条）
反应条件
1: bromobenzene With iodine; magnesium in tetrahydrofuran T=37 - 40°C; 1 h; Inert atmosphere; 2: carbon disulfide in tetrahydrofuran T=42°C; Inert atmosphere; 3: 2-bromo-2-methylpropanenitrile in tetrahydrofuran T=38 - 56°C; 25 h; Inert atmosphere;
参考文献
US2012/309900 A1, ;
Page/Page column 14 ;
反应条件
in ethyl acetate 18 h; Heating;
参考文献
Tetrahedron Letters, , vol. 40, # 12 p. 2435 - 2438
反应条件
tetraphosphorus decasulfide in toluene T=110°C; 1 h;
参考文献
Analytical Chemistry, , vol. 78, # 9 p. 3118 - 3124
反应条件
in benzene 20.5 h; Heating;
参考文献
Macromolecules, , vol. 36, # 7 p. 2256 - 2272
反应条件
in ethyl acetate 15 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 67, # 22 p. 7911 - 7914
反应条件
in toluene T=80°C; 2.5 h;
参考文献
Macromolecules, , vol. 38, # 6 p. 2033 - 2036
反应条件
1: magnesium / tetrahydrofuran / 4 h / 40 °C 2: iodine / ethyl acetate; dimethyl sulfoxide / |Darkness 3: ethyl acetate / 0.5 h / |Reflux View Scheme
参考文献
Polymer (United Kingdom), , vol. 54, # 19 p. 5122 - 5132
反应条件
in dimethyl sulfoxide; ethyl acetate T=80°C; 16 h;
参考文献
Polymer, , vol. 52, # 17 p. 3696 - 3703
反应条件
in ethyl acetate 18 h; Reflux;
参考文献
Chemistry - A European Journal, , vol. 19, # 40 p. 13317 - 13321
反应条件
1: K3Fe(CN)6 / water / 1 h 2: ethyl acetate / 18 h / Reflux View Scheme
参考文献
Journal of the Serbian Chemical Society, , vol. 75, # 12 p. 1711 - 1719
