2-三甲基甲硅烷基乙氧基羰酰氯合成路线 （共 7 条）
反应条件
potassium carbonate in toluene T=20°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 46, # 37 p. 6381 - 6384
反应条件
in toluene T=0°C; 1 h;
参考文献
Shenvi; Gerlach
Helvetica Chimica Acta, 1980 , vol. 63, # 8 p. 2426 - 2433
反应条件
triethylamine in tetrahydrofuran
参考文献
Warner-Lambert Company
Patent: US5631281 A1, 1997 ;
反应条件
triethylamine in acetonitrile 1.) 0 deg C, 15 min; 2.) room temp., overnight; Yield given;
参考文献
New River Pharmaceuticals Inc.
Patent: US6627660 B1, 2003 ;
Title/Abstract Full Text Show Details
New River Pharmaceuticals Inc.
Patent: US2004/116391 A1, 2004 ;
反应条件
sodium hydride in tetrahydrofuran T=0 - 20°C;
参考文献
Shimizu, Mamoru; Sodeoka, Mikiko
Heterocycles, 2008 , vol. 76, # 2 p. 1301 - 1312
反应条件
triethylamine in acetonitrile 1.) 0 deg C, 15 min; 2.) room temp., overnight; Yield given;
参考文献
Shute, Richard E.; Rich, Daniel H.
Synthesis, 1987 , # 4 p. 346 - 349
