1: 1-chloro-1,1-difluoro-2,2,2-trifluoroethane With n-butyllithium in diethyl ether T=-78°C; 2: chloro-diphenylphosphine in diethyl ether T=-78 - 20°C; Further stages.;
参考文献
Palcic, Jason D.; Kapoor; Roddick, Dean M.; Peters, R. Gregory
Dalton Transactions, 2004 , # 10 p. 1644 - 1647
Banger, Kulbinder K.; Brisdon, Alan K.; Herbert, Christopher J.; Ghaba, Hana Ali; Tidmarsh, Ian S.
Journal of Fluorine Chemistry, 2009 , vol. 130, # 12 p. 1117 - 1129
1: chloro-diphenylphosphine With lithium in tetrahydrofuran T=20°C; 1 h; Inert atmosphere; 2: 1-iodo-pentafluoro-ethane in tetrahydrofuran T=20°C; 1 h; Inert atmosphere;
参考文献
Banger, Kulbinder K.; Brisdon, Alan K.; Herbert, Christopher J.; Ghaba, Hana Ali; Tidmarsh, Ian S.
Journal of Fluorine Chemistry, 2009 , vol. 130, # 12 p. 1117 - 1129
