2-(苯基硫代)乙胺盐酸盐合成路线 (共 25 条)
反应条件
hydrazine hydrate in ethanol 2 h; Heating;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, p. 1956 - 1962
Zhurnal Organicheskoi Khimii, , vol. 27, # 10 p. 2210 - 2216
反应条件
lithium aluminium tetrahydride in tetrahydrofuran RefluxInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 10 p. 2386 - 2391
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 50 h; Inert atmosphere; 2: With water in tetrahydrofuran T=0°C; 0.5 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 67, # 2 p. 285 - 288
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 52 h; Inert atmosphere; 2: With water in tetrahydrofuran T=0°C; 0.5 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 67, # 2 p. 285 - 288
反应条件
potassium carbonate in dichloromethane T=20°C; 48 h;
参考文献
Journal of Organic Chemistry, , vol. 66, # 16 p. 5590 - 5594
反应条件
lithium chloride in neat (no solvent) T=130°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 57, # 23 p. 6257 - 6265
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 43, # 12 p. 2091 - 2094
反应条件
NaOPr in propan-1-ol T=6°C; Heatingvar. thiols; var solv. and reag.: NaOEt, t-BuOK, DBU; Product distribution;
参考文献
Synlett, , vol. 1997, # 8 p. 915 - 916
反应条件
triethylamine in chloroform T=0 - 5°C; 3 h;
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 15 p. 3817 - 3822
反应条件
hydrogenchloride in propionic acid 72 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1039 - 1044