3,3-二甲基-1-(2-羰基苯基)三脒合成路线 (共 10 条)
反应条件
in tetrahydrofuran Reflux;
参考文献
Okuma, Kentaro; Nojima, Akiko; Nakamura, Yuki; Matsunaga, Nahoko; Nagahora, Noriyoshi; Shioji, Kosei
Bulletin of the Chemical Society of Japan, 2011 , vol. 84, # 3 p. 328 - 332
反应条件
in dichloromethane T=0°C; 1 h; Yield given;
参考文献
Christopher Buxton; Heaney, Harry
Tetrahedron, 1995 , vol. 51, # 13 p. 3929 - 3938
反应条件
1: NO2 / 6 h / 0 °C 2: Ambient temperature View Scheme
参考文献
Elks; Hey
Journal of the Chemical Society, 1943 , p. 441,443
反应条件
gas-solid reaction; Yield given;
参考文献
Kaupp, Gerd; Herrmann, Andreas
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 3 p. 256 - 260
反应条件
in tetrahydrofuran 2 h; Reflux;
参考文献
Okuma, Kentaro; Nojima, Akiko; Nakamura, Yuki; Matsunaga, Nahoko; Nagahora, Noriyoshi; Shioji, Kosei
Bulletin of the Chemical Society of Japan, 2011 , vol. 84, # 3 p. 328 - 332
反应条件
(i) (diazotization), (ii) /BRN= 605257/, THF; Multistep reaction;
参考文献
Gompper,R. et al.
Chemische Berichte, 1968 , vol. 101, p. 2340 - 2350
反应条件
T=350°C; var. temp., also <1,6-13C2>- and <2,3-13C2>-2-(3',3'-dimethyltriazenyl)benzoic acid, and <1,6-13C2>- and <2,3-13C2>-2-aminobenzoic acid; Mechanism;
参考文献
Brown, Roger F. C.; Coulston, Karen J.; Eastwood, Frank W.; Vogel, Caspar
Australian Journal of Chemistry, 1988 , vol. 41, # 11 p. 1687 - 1696
反应条件
T=350°C; var. temp., also <1,6-13C2>- and <2,3-13C2>-2-(3',3'-dimethyltriazenyl)benzoic acid, and <1,6-13C2>- and <2,3-13C2>-2-aminobenzoic acid; Mechanism;
参考文献
Brown, Roger F. C.; Coulston, Karen J.; Eastwood, Frank W.; Vogel, Caspar
Australian Journal of Chemistry, 1988 , vol. 41, # 11 p. 1687 - 1696
参考文献
Nakayama,J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 525 - 530
反应条件
in water 2 h; Heating;
参考文献
Christopher Buxton; Heaney, Harry
Tetrahedron, 1995 , vol. 51, # 13 p. 3929 - 3938