1-(苯基乙炔基)-1-环己醇合成路线 （共 34 条）
反应条件
in tetrahydrofuran T=20 - 23°C;
参考文献
Potkin; Dikusar; Kozlov
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1260 - 1265
反应条件
1: With tetrabutyl ammonium fluoride in tetrahydrofuran T=-78°C; alkynylation; 4 h; 2: With hydrogenchloride in methanol T=0°C; Hydrolysis;
参考文献
Shibato, Atsushi; Itagaki, Yoshifumi; Tayama, Eiji; Hokke, Yasutoshi; Asao, Naoki; Maruoka, Keiji
Tetrahedron, 2000 , vol. 56, # 30 p. 5373 - 5382
反应条件
hydrogenchloride in ethanol; water Ambient temperature;
参考文献
Komissarova; Aleksandrova; Stadnichuk
Russian Journal of General Chemistry, 1997 , vol. 67, # 3 p. 412 - 416
参考文献
Journal of the American Chemical Society, , vol. 59, p. 2666
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / -78 °C 1.2: tetrahydrofuran; hexane / -78 - 20 °C 2.1: 22 percent / potassium tert-butoxide / tetrahydrofuran / 20 °C View Scheme
参考文献
Organic Letters, , vol. 7, # 22 p. 4995 - 4998
参考文献
Journal of the American Chemical Society, , vol. 53, p. 1073
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in ethanol T=70°C; 24 h;
参考文献
Catalysis Letters, , vol. 141, # 4 p. 549 - 553
反应条件
4 A molecular sieve; tetrabutyl ammonium fluoride 1.) THF; 2.) DMPU, 80 deg C, 20 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 30, # 51 p. 7149 - 7152
反应条件
potassium hydroxide anschliessendes Behandeln mit Cyclohexanon;
参考文献
Chemische Berichte, , vol. 89, p. 1775,1788
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 312, p. 1121 - 1129
