1-(3-氯苯基)-3-苯基脲合成路线 （共 13 条）
反应条件
1: benzoyl hydroxylamine With 4-methyl-morpholine; bromo-dimethylsulfonium bromide in 1,2-dichloro-ethane T=0°C; Lossen rearrangement; 2 h; Inert atmosphere; 2: 3-chloro-aniline in 1,2-dichloro-ethane T=0 - 80°C; Lossen rearrangement;
参考文献
Yadav, Deepak K.; Yadav, Arvind K.; Srivastava, Vishnu P.; Watal, Geeta; Yadav, Lal Dhar S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2890 - 2893
反应条件
thiophosgene in water; acetone Ambient temperature;
参考文献
Abuzar, Syed; Sharma, Satyavan; Iyer, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 3 p. 211 - 212
反应条件
selenium; triethylamine in toluene T=150 - 160°C; 1.5 h;
参考文献
Yang, Ying; Lu, Shiwei
Tetrahedron Letters, 1999 , vol. 40, # 26 p. 4845 - 4846
反应条件
copper acetylacetonate; potassium tert-butylate in 1-methyl-pyrrolidin-2-one T=20°C; 24 h; Inert atmosphereSealed vial;
参考文献
Gavade, Sandip; Balaskar, Ravi; Mane, Madhav; Pabrekar, Pramod N.; Mane, Dhananjay
Synthetic Communications, 2012 , vol. 42, # 11 p. 1704 - 1714
反应条件
selenium; nitrobenzene; triethylamine in toluene T=150 - 160°C; 1.5 h;
参考文献
Yang, Ying; Lu, Shiwei
Tetrahedron Letters, 1999 , vol. 40, # 26 p. 4845 - 4846
参考文献
Dondoni,A. et al.
Journal of Organic Chemistry, 1977 , vol. 42, # 21 p. 3372 - 3377
反应条件
1: (thermolysis) 2: aq. HCl View Scheme
参考文献
Dondoni,A. et al.
Journal of Organic Chemistry, 1977 , vol. 42, # 21 p. 3372 - 3377
反应条件
1: SOCl2, Et3N 2: (thermolysis) 3: aq. HCl View Scheme
参考文献
Dondoni,A. et al.
Journal of Organic Chemistry, 1977 , vol. 42, # 21 p. 3372 - 3377
参考文献
Sah
Journal of the Chinese Chemical Society (Peking), 1946 , vol. 13, p. 22,26,27
Recueil des Travaux Chimiques des Pays-Bas, 1940 , vol. 59, p. 231,233,234
Full Text Show Details
Sah; Wu
Journal of the Chinese Chemical Society (Peking), 1936 , vol. 4, p. 513,515
反应条件
1: benzene View Scheme
参考文献
Konstantinova,N.V. et al.
Journal of Organic Chemistry USSR (English Translation), 1968 , vol. 4, p. 1522 - 1526
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, p. 1583 - 1588
