2-异氰基-1,3-二异丙基苯合成路线 (共 6 条)
反应条件
diisopropylamine; trichlorophosphate in dichloromethane T=0 - 20°C; 2 h; GloveboxSchlenk techniqueInert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 135, # 29 p. 10614 - 10617
反应条件
1: tetrahydrofuran / 20 °C 2: Et3N; POCl3 / tetrahydrofuran / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 123, # 38 p. 9453 - 9454
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in toluene
参考文献
Tetrahedron Letters, , vol. 48, # 24 p. 4191 - 4193
反应条件
in toluene T=-78 - 20°C; Inert atmosphere;
参考文献
Organometallics, , vol. 29, # 23 p. 6329 - 6333
反应条件
tetrachloromethane in benzene-d6 T=20°C; Decomposition; 2 h; Photolysis; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 65, # 2 p. 624 - 626
反应条件
(i), (ii) COCl2, Et3N; Multistep reaction;
参考文献
FR1384209 , ;
Chem.Abstr., , vol. 63, # 6924