beta-L-阿拉伯糖呋喃糖合成路线 （共 4 条）
反应条件
1: 27 percent / molybdenum(VI) oxide bis-2,4-pentanedionate / dimethylformamide / 24 h / 50 °C 2: HCl / 4 h 3: 90 percent / CH2Cl2; pyridine / 3 h 4: 9.5 g / sulphuric acid, acetic acid / 15 h / 0 - 5 °C View Scheme
参考文献
Visser, G. M.; van Westrenen, J.; van Boeckel, C. A. A.; van Boom, J. H.
Recueil des Travaux Chimiques des Pays-Bas, 1986 , vol. 105, p. 528 - 537
反应条件
1: 27 percent / molybdenum(VI) oxide bis-2,4-pentanedionate / dimethylformamide / 24 h / 50 °C 2: HCl / 4 h 3: 90 percent / CH2Cl2; pyridine / 3 h 4: 9.5 g / sulphuric acid, acetic acid / 15 h / 0 - 5 °C View Scheme
参考文献
Visser, G. M.; van Westrenen, J.; van Boeckel, C. A. A.; van Boom, J. H.
Recueil des Travaux Chimiques des Pays-Bas, 1986 , vol. 105, p. 528 - 537
反应条件
1: ammonium hydroxide / methanol / 65 h / 20 °C 2: ethanol; water / 2 h / |Reflux View Scheme
参考文献
McGuigan, Christopher; Hinsinger, Karen; Farleigh, Laura; Pathirana, Ranjith N.; Bugert, Joachim J.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 3 p. 1311 - 1322
反应条件
ammonium hydroxide in methanol T=20°C; 65 h;
参考文献
McGuigan, Christopher; Hinsinger, Karen; Farleigh, Laura; Pathirana, Ranjith N.; Bugert, Joachim J.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 3 p. 1311 - 1322
