反应条件
1.1: n-BuLi / hexane; tetrahydrofuran / 0.33 h / -50 °C 2.1: 86 mg / aq. H2O2 / CHCl3 / 0.02 h 3.1: 66 percent / n-butyllithium / tetrahydrofuran; toluene / 0.5 h / -50 °C 4.1: Mg / tetrahydrofuran / 0.5 h / 20 °C 4.2: 89 percent / CuBr*Me2S / tetrahydrofuran / 0.5 h / -10 °C 5.1: 96 percent / HF/pyridine / tetrahydrofuran / 20 °C View Scheme
参考文献
Hatakeyama, Susumi; Ikeda, Tatsuhiko; Maeyama, Junji; Esumi, Tomoyuki; Iwabuchi, Yoshiharu; Irie, Hiroshi; Kawase, Akira; Kubodera, Noboru
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 22 p. 2871 - 2874
