5-氯磺酰基-2-乙氧基苯甲酸合成路线 （共 3 条）
反应条件
chlorosulfonic acid; thionyl chloride T=20°C;
参考文献
Dale, David J.; Dunn, Peter J.; Golightly, Clare; Hughes, Michael L.; Levett, Philip C.; Pearce, Andrew K.; Searle, Patricia M.; Ward, Gordon; Wood, Albert S.
Organic Process Research and Development, 2000 , vol. 4, # 1 p. 17 - 22
反应条件
1: sodium hydroxide / water / 2.08 h / 10 - 20 °C 2: ethyl acetate / 2.5 h / 55 °C / |Reflux 3: ethyl acetate / 70 h / 20 °C View Scheme
参考文献
Dale, David J.; Dunn, Peter J.; Golightly, Clare; Hughes, Michael L.; Levett, Philip C.; Pearce, Andrew K.; Searle, Patricia M.; Ward, Gordon; Wood, Albert S.
Organic Process Research and Development, 2000 , vol. 4, # 1 p. 17 - 22
反应条件
sodium hydroxide in water
T=10 - 20°C; 2.08333 h;
参考文献
Dale, David J.; Dunn, Peter J.; Golightly, Clare; Hughes, Michael L.; Levett, Philip C.; Pearce, Andrew K.; Searle, Patricia M.; Ward, Gordon; Wood, Albert S.
Organic Process Research and Development, 2000 , vol. 4, # 1 p. 17 - 22
