1,2-O-异亚丙基-alpha-D-呋喃木糖合成路线 (共 87 条)
反应条件
1: CuSO4; H2SO4 2: aq. HCl / 20 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 26, # 5-6 p. 267 - 278
反应条件
1: With sulfuric acid 2: With hydrogenchloride in water
参考文献
Nakazaki, Atsuo; Usuki, Junji; Tomooka, Katsuhiko
Synlett, 2008 , # 13 p. 2064 - 2068
反应条件
sodium tetrahydroborate in methanol T=20°C; 4 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 3 p. 551 - 557
反应条件
1: 73 percent / CuSO4, H2SO4 / CH2Cl2 / Heating 2: 90 percent / aq. HCl View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 8 p. 2600 - 2601
参考文献
Nucleosides and Nucleotides, , vol. 13, # 6-7 p. 1425 - 1452
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=60°C; 0.333333 h;
参考文献
Tetrahedron Letters, , vol. 50, # 1 p. 101 - 103
参考文献
Yamashita, Michio; Kawai, Yoshio; Uchida, Itsuo; Komori, Tadaaki; Koshaka, Masanobu; et al.
Tetrahedron Letters, 1984 , vol. 25, # 41 p. 4689 - 4692
反应条件
(+/-)-Phenyl-1,2-ethanediol; toluene-4-sulfonic acid in dichloromethane 19 h;
参考文献
Carbohydrate Research, , vol. 229, # 1 p. 141 - 148
反应条件
1: With hydrogenchloride; methanol; water 0.416667 h; 2: With sodium hydroxide in water Product distribution / selectivity;
参考文献
EP1655304 A1, ;
Page/Page column 4 ;
反应条件
1: With borane-THF in tetrahydrofuran T=20°C; 0.166667 h; Inert atmosphere; 2: With copper(II) bis(trifluoromethanesulfonate) in tetrahydrofuran 2 h; Inert atmosphere; regioselective reaction;
参考文献
Journal of the Chinese Chemical Society, , vol. 59, # 3 p. 421 - 425