1,2,4-苯并噻嗪-3-胺合成路线 （共 26 条）
反应条件
3-chloro-benzenecarboperoxoic acid in methanol; dichloromethane T=20°C; 3 h;
参考文献
EP1468688 A2, ;
Page/Page column 37; 74 ;
反应条件
3-chloro-benzenecarboperoxoic acid in methanol; dichloromethane T=20°C; 3 h;
参考文献
Magnetic Resonance in Chemistry, , vol. 44, # 10 p. 948 - 954
反应条件
dihydrogen peroxide in acetic acid T=50°C; 2 h;
参考文献
Fuchs; Chowdhury; Barnes; Gates
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 107 - 114
反应条件
1: H2O2 / acetic acid / 2 h / 50 °C 2: tert-butyl peracetate / H2O / 105 - 112 °C View Scheme
参考文献
Fuchs; Chowdhury; Barnes; Gates
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 107 - 114
反应条件
dihydrogen peroxide in acetic acid T=50°C; 2 h;
参考文献
Fuchs; Chowdhury; Barnes; Gates
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 107 - 114
反应条件
dihydrogen peroxide; acetic acid
参考文献
Fuchs; Chowdhury; Barnes; Gates
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 107 - 114
反应条件
sodium dithionite in ethanol
1 h; Heating;
参考文献
Gauthier; Duceppe
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 4 p. 1081 - 1086
反应条件
1: With potassium tert-butylate in dimethyl sulfoxide
T=20°C; 0.333333 - 0.5 h;
2: With ammonium chloride in water; dimethyl sulfoxide
参考文献
Moskalev, Nikolai V.; Gribble, Gordon W.
Patent: US2006/142569 A1, 2006 ;
Location in patent: Page/Page column 2 ;
反应条件
[bis(acetoxy)iodo]benzene in dichloromethane
T=25°C; 0.666667 h;
参考文献
Kumar, Ashok; Parshad, Mahavir; Gupta, Rakesh K.; Kumar, Devinder
Synthesis, 2009 , # 10 art. no. Z00209SS, p. 1663 - 1666
反应条件
1: With tetrabutyl ammonium fluoride in acetonitrile
T=20°C; 0.75 h; Inert atmosphere;
2: With hydrogenchloride; water in ethyl acetate; acetonitrile
参考文献
Uhde, Moritz; Ziegler, Thomas
Synthetic Communications, 2010 , vol. 40, # 20 p. 3046 - 3057
