2,2-二氟-2-苯乙腈合成路线 （共 10 条）
反应条件
P2O5 Heating1) 760 mm, 2) 10 mm;
参考文献
Middleton, W. J.; Bingham, E. M.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2883 - 2887
反应条件
IF5-5CH2Cl2 in hexane T=20°C; 2 h;
参考文献
Fukuhara, Tadahito; Hara, Shoji
Synlett, 2009 , # 2 p. 198 - 200
反应条件
diethylamino-sulfur trifluoride; zinc(II) iodide 8 h; Heating; Yield given;
参考文献
Haegele, Gerhard; Haas, Andreas
Journal of Fluorine Chemistry, 1996 , vol. 76, # 1 p. 15 - 19
反应条件
1: ZnI2 / 8 h / 100 °C 2: F3S-NEt2 / ZnI2 / 8 h / Heating View Scheme
参考文献
Haegele, Gerhard; Haas, Andreas
Journal of Fluorine Chemistry, 1996 , vol. 76, # 1 p. 15 - 19
反应条件
1: 92 percent / (diethylamino)sulfur trifluoride / Ambient temperature 2: 89 percent / NH3 / 25 °C 3: 60 percent / phosphorous pentoxide / Heating; 1) 760 mm, 2) 10 mm View Scheme
参考文献
Middleton, W. J.; Bingham, E. M.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2883 - 2887
反应条件
1: 89 percent / NH3 / 25 °C 2: 60 percent / phosphorous pentoxide / Heating; 1) 760 mm, 2) 10 mm View Scheme
参考文献
Middleton, W. J.; Bingham, E. M.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2883 - 2887
参考文献
Jagupol'skii; Belinskaja
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 772,774; engl. Ausg. S. 750, 752
反应条件
1: concentrated H2SO4 2: aqueous NaOH View Scheme
参考文献
Jagupol'skii; Belinskaja
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 772,774; engl. Ausg. S. 750, 752
反应条件
1: concentrated H2SO4 2: aqueous NaOH 3: SOCl2 View Scheme
参考文献
Jagupol'skii; Belinskaja
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 772,774; engl. Ausg. S. 750, 752
参考文献
Jagupol'skii; Belinskaja
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 772,774; engl. Ausg. S. 750, 752
