反应条件
1: 17 percent / Na2CO3 / H2O; tetrahydrofuran / 1.5 h / Ambient temperature 2: 1.) ClC(S)OPh, NaHCO3, 2.) Et3N / 1.) THF, H2O, room temperature, 15 h, 2.) MeOH, room temperature, 22 h 3: 1.) LiOH*H2O, 2.) HCl / 1.) THF, H2O, room temperature, 18 h, 5.) CH2Cl2, room temperature, 15 min View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 20 p. 6296 - 6301
